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A microwave-assisted route for the solid-state synthesis of lead pyrophosphate, Pb2P2O7

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Abstract

In this study, we have developed a new method based on microwave heating for the preparation of lead pyrophosphate compound, Pb2P2O7. The favoring of microwave heating as synthesis technique is based on the fact being much faster, cleaner and economical than conventional techniques. By following this new route, the lead pyrophosphate, Pb2P2O7, was obtained as a pure phase. The products were characterized by X-ray powder diffraction (XRD) and Fourier Transform IR (FTIR) spectroscopic techniques. Comparing the experimental XRD and FTIR data of the synthesized products with the reported literature data has revealed that there was mutually an excellent agreement.

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Authors and Affiliations

  1. Department of Chemistry, Science Faculty, Balikesir University, 10100, Balikesir, Turkey

    Halil Guler & Figen Kurtulus

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  1. Halil Guler
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  2. Figen Kurtulus
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Correspondence to Halil Guler.

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Guler, H., Kurtulus, F. A microwave-assisted route for the solid-state synthesis of lead pyrophosphate, Pb2P2O7. J Mater Sci 40, 6565–6569 (2005). https://doi.org/10.1007/s10853-005-1809-y

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  • DOI: https://doi.org/10.1007/s10853-005-1809-y

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