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Structural Elucidation of {[(CH3)2SnCl2·H2O]2·18-crown-6} n and its Hydrogen Bonding in Solution by HMBC Spectroscopy

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Abstract

Behavior of {[(CH3)2SnCl2·H2O]2·18-crown-6} n in solution have been investigated by HMBC NMR. The results show that coordination of water to tin containing species and its hydrogen bonding to crown ether remains intact in non-coordinating solvent in contrast to coordinating solvent. H-NMR reveals that the chemical shift of water in complex varies by solvent of crystallization.

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Authors and Affiliations

  1. Department of chemistry, Shahid Beheshti University, 1983963113, Tehran, Iran

    Mostafa M. Amini, Amirreza Azadmher & Hamid Reza Bijanzadeh

  2. Department of chemistry, Trabit Modaress University, Tehran, Iran

    Nasser Hadipour

Authors
  1. Mostafa M. Amini
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  2. Amirreza Azadmher
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  3. Hamid Reza Bijanzadeh
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  4. Nasser Hadipour
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Correspondence to Mostafa M. Amini.

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Amini, M.M., Azadmher, A., Bijanzadeh, H.R. et al. Structural Elucidation of {[(CH3)2SnCl2·H2O]2·18-crown-6} n and its Hydrogen Bonding in Solution by HMBC Spectroscopy. J Incl Phenom Macrocycl Chem 54, 77–80 (2006). https://doi.org/10.1007/s10847-005-4560-8

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  • DOI: https://doi.org/10.1007/s10847-005-4560-8

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