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Influence of synthesis method on the properties of mixed Aurivillius phase Bi5TiNbWO15

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Abstract

The ceramic material Bi5TiNbWO15 (BTNW) was obtained and is characterized by a layered, Aurivillus type structure (MBLPO—mixed bismuth oxide layered perovskites) with m = 1.5. In order to optimize the production, BTNW was synthesized by two methods: synthesis of a mixture of simple oxides Bi2O3, Nb2O5, WO3, TiO2 and synthesis of a mixture of appropriate, layered Aurivillus type structures Bi2WO6 (m = 1) and Bi3TiNbO9 (m = 2). Synthesized solid solutions were consolidated with a conventional method. The crystal structure of Bi2WO6 and Bi3TiNbO9 Bi5TiNbWO15 was examined at room temperature with an X-ray diffraction method. Microstructure and chemical composition were analyzed. The authors analyzed the temperature—permittivity ɛ relationship for the ceramic with m = 1,5, which was obtained with two methods, as well as for m = 1 and m = 2.

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Acknowledgements

The financial support for this work was provided by the Ministry of Science and Higher Education, Poland, under grant no. N50714231/3568 (2006–2009).

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Authors and Affiliations

  1. Department of Material Science, University of Silesia, Zeromski St 3, 41-200, Sosnowiec, Poland

    Dorota Machura & Zygmunt Surowiak

  2. Institute of Material Science, University of Silesia, Katowice, Poland

    Pawel Pacek

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  1. Dorota Machura
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  2. Zygmunt Surowiak
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  3. Pawel Pacek
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Correspondence to Dorota Machura.

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Machura, D., Surowiak, Z. & Pacek, P. Influence of synthesis method on the properties of mixed Aurivillius phase Bi5TiNbWO15 . J Electroceram 19, 215–220 (2007). https://doi.org/10.1007/s10832-007-9319-8

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  • DOI: https://doi.org/10.1007/s10832-007-9319-8

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