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Analysis of Nitropolycyclic Aromatic Hydrocarbons in Fine Particulate Matter by Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry Using Fe3O4/ZIF-8 Magnetic Nanocomposites as Matrix

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Journal of Applied Spectroscopy Aims and scope

Core-shell magnetic metal organic nanocrystals were synthesized and used as matrix for matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS). Four nitropolycyclic aromatic hydrocarbons (nitro-PAHs) were successfully detected by using negative-ion MALDI-TOF MS without background interference. Furthermore, the magnetic nanocomposites (MNCs) coated with zeolitic imidazolate framework-8 (ZIF-8) showed excellent adsorption and enrichment capacity, and can be isolated with a magnet and directly spotted on the stainless steel plate for MALDI measurement. It was also analyzed nitro-PAHs in PM2.5 samples using the ZIF-8-coated magnetic nanocomposite as adsorbent and matrix.

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Authors and Affiliations

  1. School of Basic Medical Science, Shanxi Medical University, Taiyuan, 030001, China

    Haojiang Wang, Wei Bian, Tijian Sun & Jiancong Wei

  2. College of Pharmacy, Shanxi Medical University, Taiyuan, 030001, China

    Xuan Wang

  3. Hong Kong Baptist University, State Key Laboratory of Environmental and Biological Analysis, Hong Kong, SAR, China

    Zongwei Cai

Authors
  1. Haojiang Wang
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  2. Xuan Wang
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  3. Wei Bian
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  4. Tijian Sun
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  5. Zongwei Cai
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  6. Jiancong Wei
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Corresponding author

Correspondence to Wei Bian.

Additional information

Published in Zhurnal Prikladnoi Spektroskopii, Vol. 86, No. 1, pp. 103–109, January–February, 2019.

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Wang, H., Wang, X., Bian, W. et al. Analysis of Nitropolycyclic Aromatic Hydrocarbons in Fine Particulate Matter by Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry Using Fe3O4/ZIF-8 Magnetic Nanocomposites as Matrix. J Appl Spectrosc 86, 89–95 (2019). https://doi.org/10.1007/s10812-019-00786-5

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  • DOI: https://doi.org/10.1007/s10812-019-00786-5

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