Abstract
The sound velocity of Sedlec kaolin during heating from 20 °C to 1100 °C was investigated by modulated force thermomechanical analysis (mf-TMA). In the interval from 20 °C to 250 °C, the sound velocity increases which can be explained by liberation of the water molecules from pores and micropores. Dehydroxylation (450 °C to 650 °C) presents itself with a decrease of the sound velocity. After dehydroxylation, a two-step increase of the sound velocity was observed. The first step of the increase of the sound velocity is due to solid-state sintering at low temperatures. The second step starts at 950 °C as a consequence of the collapse of the metakaolinite structure. After the maximum, a steep increase of the sound velocity follows as a result of solid-state sintering.
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Trník, A., Štubňa, I. & Moravčíková, J. Sound Velocity of Kaolin in the Temperature Range from 20 °C to 1100 °C. Int J Thermophys 30, 1323–1328 (2009). https://doi.org/10.1007/s10765-009-0634-y
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DOI: https://doi.org/10.1007/s10765-009-0634-y