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Evolution of synchrotron-radiation-based Mössbauer absorption spectroscopy for various isotopes

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Abstract

Synchrotron-radiation-based Mössbauer spectroscopy that yields absorption type Mössbauer spectra has been applied to various isotopes. This method enables the advanced measurement by using the excellent features of synchrotron radiation, such as Mössbauer spectroscopic measurement under high-pressures. Furthermore, energy selectivity of synchrotron radiation allows us to measure 40K Mössbauer spectra, of which observation is impossible by using ordinary radioactive sources because the first excited state of 40K is not populated by any radioactive parent nuclides. Moreover, this method has flexibility of the experimental setup that the measured sample can be used as a transmitter or a scatterer, depending on the sample conditions. To enhance the measurement efficiency of the spectroscopy, we developed a detection system in which a windowless avalanche photodiode (APD) detector is combined with a vacuum cryostat to detect internal conversion electrons adding to X-rays accompanied by nuclear de-excitation. In particular, by selecting the emission from the scatterer sample, depth selective synchrotron-radiation-based Mössbauer spectroscopy is possible. Furthermore, limitation of the time window in the delayed components enables us to obtain narrow linewidth in Mössbauer spectra. Measurement system that records velocity dependent time spectra and energy information simultaneously realizes the depth selective and narrow linewidth measurement.

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Acknowledgements

This work was supported by JSPS KAKENHI Grant-in-Aid for Scientific Research (S) of Grant No. 24221005. The experiments at SPring-8 were performed with the approval of the Japan Synchrotron Radiation Research Institute (JASRI) (2009A0086, 2017A3581).

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Authors and Affiliations

  1. Research Reactor Institute, Kyoto University, Kumatori-cho, Sennan-gun, Osaka, 590-0494, Japan

    Makoto Seto, Ryo Masuda, Yasuhiro Kobayashi, Shinji Kitao, Masayuki Kurokuzu, Makina Saito, Shuuich Hosokawa & Hiroki Ishibashi

  2. National Institutes for Quantum and Radiological Science and Technology, Sayo-cho, Sayo-gun, Hyogo, 679-5148, Japan

    Takaya Mitsui

  3. Resarch and Utilization Division, Japan Synchrotron Radiation Research Institute, Sayo-cho, Sayo-gun, Hyogo, 679-5198, Japan

    Yoshitaka Yoda

  4. Nagoya Institute of Technology, Gokiso-cho, Showa-ku, Nagoya, Aichi, 466-8555, Japan

    Ko Mibu

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  1. Makoto Seto
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  2. Ryo Masuda
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  3. Yasuhiro Kobayashi
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  4. Shinji Kitao
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  5. Masayuki Kurokuzu
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  9. Takaya Mitsui
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  10. Yoshitaka Yoda
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  11. Ko Mibu
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Correspondence to Makoto Seto.

Additional information

This article is part of the Topical Collection on Proceedings of the International Conference on the Applications of the Mössbauer Effect (ICAME 2017), Saint-Petersburg, Russia, 3-8 September 2017

Edited by Valentin Semenov

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Seto, M., Masuda, R., Kobayashi, Y. et al. Evolution of synchrotron-radiation-based Mössbauer absorption spectroscopy for various isotopes. Hyperfine Interact 238, 78 (2017). https://doi.org/10.1007/s10751-017-1446-2

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  • DOI: https://doi.org/10.1007/s10751-017-1446-2

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