A comparative investigation was performed on the possibility of controlling the average sizes of nano-sized powders of silicon dioxide and aluminum oxide, obtained by electron-beam evaporation and by pyrogenic, liquid chemical, and plasma chemical methods, by keeping them in the temperature range 800 – 1300°C in an air atmosphere. The average sizes of the resulting particles were estimated from measurements of the specific surface area using the Brunauer–Emmett–Taylor (BET) adsorption method at liquid nitrogen temperature. The crystallographic parameters in the treated powders were assessed by means of x-ray diffraction analysis. It is shown that by making a suitable choice of temperatures and initial powder it is possible to achieve in the resulting powder the phase composition and an average particle size close to a specified value.
Similar content being viewed by others
References
Kenneth J. Klabunde and Ryan M. Richards (eds.), Nanoscale Materials in Chemistry, A John Wiley and Sons, Hoboken (2009).
Ya. E. Geguzin, The Physics of Sintering [in Russian], Nauka, Moscow (1984).
V. N. Antsiferov and V. E. Perelman, Mechanics of Pressing of Powder and Composite Materials [in Russian], Graal’, Moscow (2001).
M. K. Berner, V. E. Zarko, and M. B. Talavar “Nanoparticles of energetic materials: preparation methods and properties (review),” Fiz. Goreniya Vzryva, 49(6), 3 – 30 (2013).
S. P. Bardakhanov, V. Z. Gindulina, and V. A. Lienko, “Possible uses of nanodispersed powders in ceramic production,” in: Abstracts of Reports at the 5th All-Russia Conf. on the Physicochemistry of Ultradisperse Systems [in Russian], Ekaterinburg (2000), pp. 371 – 372.
S. P. Bardakhanov, V. Z. Gindulina, and V. A. Lienko, “Preparation of ceramic materials based on nanodispersed powders,” in: Reports of the Scientific-Practical Conf. of the Materials Science Societies of Russia on ‘New Structural Materials,’ Zvenigorod (2000), pp. 161 – 162.
C. Bae, S. Bardakhanov, J. Chong, et al., “Ceramic preparation of nano- and micropowder,” in: Abstracts of the 9th Intern. Symp. on Metastable, Mechanically Alloyed and Nanocrystalline Materials, Seoul, Korea (2002).
S. P. Bardakhanov, A. V. Kim, V. A. Lienko, et al., “Experimental study on the creation of environmentally friendly technology for producing ceramics from nanodispersed powders,” Konstr. Kompozit. Nanodispers. Mater. VIMI, No. 4, 71 – 79 (2005).
M. I. Alymov, “Structural powder materials,” Kompozity i Nanostruktury, No. 2, 5 – 11 (2010).
O. L. Khasanov, Yu. P. Pokholkov, V. M. Sokolov, et al., “Ultrasonic compaction of zirconium ceramics from ultrafine powders,” Glass Ceram., 52(7), 177 – 180 (1995).
R. Eiler, Chemistry of Silica [Russian translation], Mir, Moscow (1982).
V. P. Lukashov, S. P. Bardakhanov, R. A. Salimov, etc. Pat. RF 2067077, IPC S01B 33/18. Method for Producing Ultrafine Silicon Dioxide, a Device for Its Implementation and Ultrafine Silicon Dioxide [in Russian], publ. 09.27.1996.
S. P. Bardakhanov, “The formation of fine silica powder after vaporization of quartz,” Computer Aided Design of Advanced Materials and Technologies (CADAMT’97): Abstracts of the 5th International Conference. Baikal Lake, Russia, Tomsk, 4 – 6 August 1997 [in Russian], Tomsk (1997), pp. 88 – 89.
S. P. Bardakhanov, A. I. Korchagin, N. K. Kuksanov, et al. “Nanopowder production based on technology of solid raw substances evaporation by electron beam accelerator,” Mat. Sci. Eng., 132(1 – 2), 204 – 208 (2006).
S. P. Bardakhanov, A. I. Korchagin, N. K. Kuksanov, et al., “Preparation of nanopowders by evaporation of starting substances in an electron accelerator at atmospheric pressure,” Dokl. Akad. Nauk, 409(3), 320 – 323 (2006).
J. Mathias and G. Wannemacher, “Basic characteristics and applications of aerosil: 30. The chemistry and physics of the aerosil surface,” J. Colloid Interface Sci., 125(1), September, 61 – 68 (1988).
Technical Overview 13 – AEROXIDE® Fumed Metal Oxides, Evonik Industries (2017).
Shinji Fujiwara, Yasuaki Tamura, Hajime Maki, et al. “Development of new high-purity aluminum,” Sumitomo Kagaku R&D Reports (English Edition), 2007-I(2007.5.31), 1 – 10 (2007). URL: https://www.sumitomo-chem.co.jp/english/rd/report/files/docs/03_2007-1e.pdf
Website of the Chinese Company XFNANO, URL: https://www.xfnano.com/product/detail?goodId= (access date: 09/11/2023).
V. K. Larin, V. M. Kondakov, E. N. Maly, et al., “Plasmochemical method for producing ultrafine (nano-) powders of metal oxides and promising directions for their application,” Izv. Vyssh. Ucheb. Zaved., Tsvetn. Met., No. 5, 59 – 64 (2003).
N. V. Dedov, E. M. Kutyavin, A. M. Selikhovkin, et al., Structure and Properties of Nanodispersed Aluminum Oxide Powders Obtained by Plasma-Chemical Method, URL: https://textarchive.ru/c-2971290.html (access date: 09/11/2023).
L. S. Vikulina, “Determination of the fractal dimension of nanopowders by the method of area and perimeter ratio,” Design and Technology of Electronic Means, No. 4, 2 – 6 (2013).
S. P. Bardakhanov, L. S. Vikulina, V. I. Lysenko, et al., “Analysis of nanopowders by small-angle x-ray scattering,” Vest. Novosibirsk. Gos. Univ., Ser. Fiz., 7(4), 107 – 116 (2012).
V. V. Syzrantsev, L. S. Vikulina, S. P. Bardakhanov, A. V. Nomoev, et al., “The different fractal structure of oxide nanopowders depending on the method of production,” Solid State Phenom., 271, 124 – 132 (2018). DOI: https://doi.org/10.4028/www.scientific.net/SSP.271.124
A. P. Zav’yalov, V. V. Syzrantsev, K. V. Zobov and S. P. Bardakhanov, “Influence of agglomeration on the viscosity of nanofluids,” J. Eng. Phys. Thermophys., 91(1), 115 – 123 (2018). DOI https://doi.org/10.1007/s10891-018-172
Y. A. Abzaev, V. V. Syzrantsev, and S. P. Bardakhanov, “Simulation of the structural state of amorphous phases in nanoscale SiO2 synthesized via different methods,” Phys. Solid State, No. 59(9), 1874 – 1878 (2017). DOI: https://doi.org/10.1134/S1063783417090025
U. A. Abzaev, V. V. Syzrantsev, and S. P. Bardakhanov, “Modeling of the structural state of amorphous phases of the nano-sized Al2O3 produced by different synthesis methods,” Russian Phys. J., No. 60(3), 522 – 528 (2017). DOI: https://doi.org/10.1007/s11182-017-1103-x
S. P. Bardakhanov, I. V. Vasiljeva, N. K. Kuksanov, and S. V. Mjakin, “Surface functionality features of nanosized silica obtained by electron beam evaporation at ambient pressure,” Adv. Mater. Sci. Eng., 2010, 241,695 – 241,699 (2010).
V. Syzrantsev, E. Paukshtis, T. Larina, et al., “Features of surface structures of alumina and titanium dioxide nanoparticles produced using different synthesis methods,” J. Nanomater., 2018, Art. No. 2065687, 1 – 10 (2018). DOI: https://doi.org/10.1155/2018/2065687
D. Yu. Trufanov, “Study of the properties of ceramics based on Tarkosil T-20 powder depending on their maximum sintering temperature [Electronic resource],” in: II International Forum on Nanotechnologies (Rusnanotech 2009): Coll. Abstracts of Reports of Participants in the Competition of ScientificWorks of Young Scientists, Moscow, October 6 – 8, 2009 [in Russian], RUSNANO, Moscow (2009), pp. 81 – 82.
V. V. Storozh, G. Ya. Akimov, I. V. Gorelik, and N. G. Labinskaya, “Study of polymorphic transformations in aluminum oxide I. Experiment,” Zh. Tekh. Fiz., 9, 86 – 97 (1996).
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Steklo i Keramika, No. 10, pp. 10 – 20, October, 2023.
Rights and permissions
Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
About this article
Cite this article
Gaponenko, V.R., Bardakhanov, S.P. & Trufanov, D.Y. Temperature Influence on the Properties of Freely Poured Nano-Sized Inorganic Oxide Powders. Glass Ceram 80, 409–416 (2024). https://doi.org/10.1007/s10717-023-00624-3
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10717-023-00624-3