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The Nucleation Effect of PbSe Additive on Bi2Sr2CaCu2Oδ Glass Ceramics

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The crystallisation kinetics and effects of doping on Bi2Sr2CaCu2Oδ (BSCCO) glass ceramic system with 0.0%, 0.1%, 0.3% and 0.5% PbSe were investigated in this study. Differential thermal analysis (DTA) was used to investigate the effects of PbSe doping on glass transition, nucleation and crystallisation temperature of glass were investigated. The DTA results were analysed using the Ozawa, Augis–Bennett, Takhor and Kissinger equations for nucleation kinetics to determine the activation energies and Avrami parameters. Thermogravimetric analysis revealed that the amount of oxidation in the structure increased with increasing PbSe-doping concentration.

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The authors acknowledge financial support for this work through the Scientific Research Projects (BAP 05/2011-48) Foundation of Gazi University Ankara.

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Authors and Affiliations

  1. Gazi University, Faculty of Sciences, Department of Physics, 06531, Ankara, Turkey

    Şükrü Çavdar, Emre Deniz, Neslihan Turan & Ahmet Tolga Taşçı

  2. Department of Electrical and Electronics Engineering, Faculty of Engineering and Architecture, Kastamonu University, 37100, Kastamonu, Turkey

    Özgür Öztürk & Haluk Koralay

Authors
  1. Şükrü Çavdar
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  2. Emre Deniz
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  3. Neslihan Turan
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  4. Ahmet Tolga Taşçı
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  5. Özgür Öztürk
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  6. Haluk Koralay
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Correspondence to Neslihan Turan.

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Abstract published in Steklo i Keramika, No. 2, pp. 47 – 48, February, 2022.

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Çavdar, Ş., Deniz, E., Turan, N. et al. The Nucleation Effect of PbSe Additive on Bi2Sr2CaCu2Oδ Glass Ceramics. Glass Ceram 79, 75–81 (2022). https://doi.org/10.1007/s10717-022-00458-5

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  • DOI: https://doi.org/10.1007/s10717-022-00458-5

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