The results of studies of the microstructure, phase state, and physicomechanical properties of 3 μm thick Al–Si–N and Zr–Y–O coatings obtained by pulsed magnetron sputtering on the surface of single-crystal m-Si are reported. It was found that for Al–Si–N and Zr–Y–O coatings the light transmittance in the visible range of the spectrum reaches 83 and 78%, respectively. It was shown that the crack resistance of m-Si samples with protective coatings is two to three times higher than that for the initial silicon samples. The results of laboratory tests of the resistance of the samples to impact loads on interaction with a flow of high-speed (5 – 7 km/sec) solid microparticles of Fe showed that 3 μm thick protective coatings on m-Si samples makes it possible to suppress surface erosion of the latter by preventing the formation of fine craters.
Similar content being viewed by others
References
E. Lewin, D. Loch, A. Montagne, et al., “Comparison of Al–Si–N nanocomposite coatings deposited by HIPIMS and DC magnetron sputtering,” Surf. Coat. Technol., 232, 680 – 689 (2013).
A. M. Telegin and N. D. Semkin, Cosmic Dust and Its Interaction with Spacecraft [in Russian], Izd. SGAU, Samara (2015).
I. A. Bozhko, E. V. Rybalko, M. V. Fedorischeva et. al., “Protection from high-speed impact particles for quartz glass by coatings on the basis of Al–Si–N,” AIP Conf. Proc., 1783, 020018 (1 – 4) (2016).
V. P. Sergeev, V. P. Yanovsky, Yu. N. Paraev, et al., “Installation of ion-magnetron sputtering of nanocrystalline coatings (QUANTUM),” Phys. Mesomekh., 7(2) (special issue), 333 – 336 (2004).
B. R. Lawn, A. G. Evans, and D. B. Marshall, “Elastic/plastic indentation damage in ceramics: the median/radial crack system,” J. Am. Ceram. Soc., 63, 574 – 581 (1980).
A. Useinov, K. Kravchuk, and I. Maslenikov, “Indentation. Measurement of hardness and crack resistance of coatings,” Nanoindustriya, No. 7, 48 – 56 (2013).
G. R. Anstis, P. Chantikul, B. R. Lawn, and D. B. Marshall, “A critical evaluation of indentation techniques for measuring fracture toughness. I. Direct crack measurements,” J. Am. Ceram. Soc., 64, 533 – 538 (1981).
G. A. Rokhin, V. V. Zharovtsev, S. V. Sinyaev, et al., “Light-gas accelerators and physical modeling of high-speed collisions of solids at cosmic speeds in laboratory conditions,” Dokl. Akad. Nauk, 402(2), 197 – 200 (2005).
A. V. Gerasimov, M. P. Kalashnikov, V. P. Sergeev, et al., “Complex research on the interaction of glass with space debris,” AIP Conf. Proc., 1683, 020056 (2015).
This work was performed as part of the program of fundamental scientific research of state academies of science for the years 2013 – 2020, direction III.23. ‘Laboratory tests for the effect of impacts of solid microparticles on the studied samples’ performed under RSF grant 16-19-10264.
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Steklo i Keramika, No. 4, pp. 37 – 43, April, 2020.
Rights and permissions
About this article
Cite this article
Bozhko, I.A., Kalashnikov, M.P., Fedorishcheva, M.V. et al. Development and Study of the Properties of Impact-Resistant Ceramic Nanocomposite Coatings for Silicon. Glass Ceram 77, 149–153 (2020). https://doi.org/10.1007/s10717-020-00259-8
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10717-020-00259-8