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IR Spectral Study and X-Ray Structural Analysis of the Supramolecular Structure of Cellulose Powder

  • RESEARCH METHODS
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Fibre Chemistry Aims and scope

IR spectroscopy and x-ray structural analysis were used to study the supramolecular structure of cellulose powders obtained by the hydrolytic decomposition of bleached coniferous cellulose using mineral acids and its mercerized form. IR spectroscopy was used to establish the nature of the intermolecular bonds in the cellulose powder macromolecules. The Rietveld refinement was used to determine crystallinity and size of coherent scattering regions as well as to calculate the lattice periods of the crystalline component of these materials.

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This work was carried out employing equipment of the Chemistry Collective Use Center at the Institute of Chemistry, Urals Branch, Russian Academy of Science.

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Authors and Affiliations

  1. Institute of Chemistry, Komi Science Center, Urals Branch of the Russian Academy of Science, Syktyvka, Russia

    E. G. Kazakova, E. U. Ipatova & E. V. Udoratina

  2. Petrozavodsk State University, Petrozavodsk, Russia

    L. A. Aleshina & L. A. Lugovskaya

  3. Syktyvkar Forest Institute, Syktyvka, Russia

    V. A. Demin

Authors
  1. E. G. Kazakova
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  2. L. A. Aleshina
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  3. L. A. Lugovskaya
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  4. V. A. Demin
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  5. E. U. Ipatova
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  6. E. V. Udoratina
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Corresponding author

Correspondence to E. G. Kazakova.

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Translated from Khimisheskie Volokna, Vol. 48, No. 4, pp. 85-92, July-August, 2016.

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Kazakova, E.G., Aleshina, L.A., Lugovskaya, L.A. et al. IR Spectral Study and X-Ray Structural Analysis of the Supramolecular Structure of Cellulose Powder. Fibre Chem 48, 342–348 (2016). https://doi.org/10.1007/s10692-017-9794-x

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  • DOI: https://doi.org/10.1007/s10692-017-9794-x

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