Skip to main content
SpringerLink
Log in

Purity of Monomers for Manufacturing Aramid Fibers Measured by Differential Scanning Calorimetry

  • RESEARCH METHODS
  • Published:
Fibre Chemistry Aims and scope

A differential scanning calorimetric method for measuring the purity of thermally stable monomers used to manufacture aramid threads with a distinctly defined melting point is described. The thermal regimes for analyzing various organic substances are developed. A method for calculating the absolute amount of impurities using thermograms is proposed. It is based on plots of the fraction of melted sample as a function of melting point. A stepwise procedure for measuring the purity for practical utilization is developed. Examples of the calculation of the purity of various substances are given.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. ASTM Standard E-928 “Standard Test Method for Purity by Differential Scanning Calorimetry.”

  2. C. Plato and S. R. Glasgow, J. Anal. Chem., 41, No. 2, 330 (1969).

    Article  CAS  Google Scholar 

  3. USER COM, information for users of Mettler Toledo Thermal Analysis Systems, 10, 2/99.

  4. A. L. Emelina, Differential Scanning Calorimetry [in Russian], Lab. Khim. Fak. MGU, 2009.

  5. A. A. S. Araujo, M. dos Santos Bezerra, et al., Braz. J. Pharm. Sci., 46, No. 1, 37-43 (2010).

    Article  Google Scholar 

  6. W. J. Sichina, PETech-30 Thermal Analysis, Perkin Elmer Inc., 2000.

  7. G. B. Sklyarova, “Development of physicochemical analytical and control methods for process solutions in the manufacture of aramid fibers” [in Russian], Candidate Dissertation in Chemical Sciences, May 17, 2006, MGTU, Moscow, 2007, 112 pp.

  8. M. V. Shablygin, G. B. Sklyarova, and S. V. Komissarov, Khim. Volokna, No. 1, 59-63 (2012).

Download references

Author information

Authors and Affiliations

  1. Kamenskvolokno Corp., 347800, Kamensk-Shakhtinskii, 1 Saprygina St., Russia

    A. S. Shraifel’, S. V. Komissarov & G. B. Sklyarova

Authors
  1. A. S. Shraifel’
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. S. V. Komissarov
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. G. B. Sklyarova
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to A. S. Shraifel’.

Additional information

Translated from Khimicheskie Volokna, No. 4, pp. 58-61, July—August, 2014.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Shraifel’, A.S., Komissarov, S.V. & Sklyarova, G.B. Purity of Monomers for Manufacturing Aramid Fibers Measured by Differential Scanning Calorimetry. Fibre Chem 46, 262–265 (2014). https://doi.org/10.1007/s10692-014-9602-9

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10692-014-9602-9

Keywords

Search

Navigation