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Potentiometric determination of the content of water-soluble organic amides

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Abstract

A method was developed for determining water-soluble, nitrogen-containing organic compounds based on their potentiometric titration with a polarized platinum microelectrode in HCl medium with a solution of tungstophosphoric heteropolyacid. The range of determinable concentrations is 0.4–65%. The method is characterized by good reproducibility (Sr no greater than 0.02–0.04) both for model and for process solutions. The duration of the analysis to determine the DMAA content using tungstophosphoric heteropolyacid is a maximum of 15 min.

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References

  1. I. A. Zhironkina, V. V. Bogoslovskii, and S. G. Mairanovskii, Elektrokhimiya, 26, No. 8, 1045 (1990).

    CAS  Google Scholar 

  2. V. V. Bogoslovskii, Ya. Ya. Makarov-Zemlyanskii, and N. V. Bogdanov, in: Proceedings of the I International Forum “Analysis and Analytics” [in Russian], Vol. 1, Voronezh (2003), p. 220.

    Google Scholar 

  3. I. Gyenes, Titration in Nonaqueous Media, Akademiai K, Budapest (1970).

    Google Scholar 

  4. P. K. Agasyan and E. R. Nikolaeva, Principles of Electrochemical Methods of Analysis [in Russian], MGU, Moscow (1986).

    Google Scholar 

  5. L. N. Lebedeva and D. N. Nikolaeva, Heteropolycompounds in Analytical Chemistry. Problems of Modern Analytical Chemistry [in Russian], No. 4, Nauka, Moscow (1983), pp. 142–146.

    Google Scholar 

  6. V. V. Bogoslovskii and I. P. Pizelkin, Zh. Anal. Khim., 61, No. 9, 901 (2006).

    Google Scholar 

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Translated from Khimicheskie Volokna, No. 1, pp. 55–57, January–February, 2007.

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Bogoslovskiy, V.V., Chernova, N.S. Potentiometric determination of the content of water-soluble organic amides. Fibre Chem 39, 73–75 (2007). https://doi.org/10.1007/s10692-007-0017-8

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  • DOI: https://doi.org/10.1007/s10692-007-0017-8

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