A new thiophene acetylene, named 2,2-dimethyl-4-[5′-(prop-1-ynyl)-2,2′-bithiophen-5-yl]-1,3-dioxolane (1), was isolated from the roots of Echinops spinosus, and the structure was elucidated on the basis of oneand two-dimensional NMR (including 1H, 13C NMR, DEPT, 1H–1H COSY, HSQC, and HMBC).
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Acknowledgment
We are grateful for financial support from the National Natural Science Foundation of China (81602978), the Hebei Medical University Development Project (2016-kyfz111), and the Natural Science Foundation of Hebei Province (H2017206087). We also wish to extend our sincere thanks for the financial support of Syngenta Ltd. (2016-Hebei Medical University-Syngenta-05).
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Published in Khimiya Prirodnykh Soedinenii, No. 5, September–October, 2017, pp. 796–797.
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Wu, Y., Li, S., Zhang, Z. et al. New Thiophene Acetylene from Echinops spinosissimus subsp. spinosus . Chem Nat Compd 53, 933–934 (2017). https://doi.org/10.1007/s10600-017-2158-1
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DOI: https://doi.org/10.1007/s10600-017-2158-1