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Phosphorylation of technical lignins

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Chemistry of Natural Compounds Aims and scope

A method for phosphorylation of technical lignins and their derivatives by the action of thiophosphoryl chloride on air-dried sodium lignates over 5–30 min with vigorous stirring and simultaneous grinding in a solvent-free vibrating reactor at 20–80 °C followed by alkali-metal alkoxides with vigorous stirring and simultaneous grinding for 10–40 min at the same temperature and a 1:1 mole ratio of phosphorylating reagents calculated per mole of lignin OH groups was developed.

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References

  1. L. A. Pershina, “Reaction of Lignins with Organophosphorus Compounds,” Doctoral Dissertation, IWC, AS Latv. SSR, Riga, 1972.

  2. B. V. Tronov, L. A. Pershina, V. M. Morozova, and A. I. Galochkin, Gidrol. Lesokhim. Promst., 5, 12 (1961).

    Google Scholar 

  3. L. A. Pershina, A. I. Galochkin, and G. G. Lykhina, Khim. Drev., 1, 325 (1968).

    CAS  Google Scholar 

  4. L. G. Shen, Khim. Rastit. Syryya, 2, 57 (2000).

    Google Scholar 

  5. A. I. Galochkin, L. A. Pershina, and L. G. Shen, RF Pat. No. 2,194,710 (2002); Byull. Izobret., No. 35 (2002).

  6. G. Shrader, Usp. Khim., 22(6), 712 (1953).

    Google Scholar 

  7. A. I. Galochkin, I. V. Ananyina, and M. V. Efanov, RF Pat. No. 2,371,446 (2009); Byull. Izobret., No. 30 (2009).

  8. T. V. Izumrudova and E. A. Demyyanova, Reagents from Lignin, Physicochemical Rationale for Their Use [in Russian], TsNIITEIlesprom, Moscow, 1968.

    Google Scholar 

  9. V. A. Klimova, Basic Analytical Micromethods for Organic Compounds [in Russian], Khimiya, Moscow, 1975.

    Google Scholar 

  10. Methodical Instructions No. 3.5.2.1759-03, Methods for Determining the Effectiveness of Insecticides Used in Medical Pest Control, RF Min. Health, Moscow, 2003.

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Authors and Affiliations

  1. High Technology Technopark, 628011, Russia, Khanty-Mansiisk, Ul. Studencheskaya, 27

    M. V. Efanov & A. I. Galochkin

Authors
  1. M. V. Efanov
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  2. A. I. Galochkin
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Correspondence to M. V. Efanov.

Additional information

Deceased (A. I. Galochkin).

Translated from Khimiya Prirodnykh Soedinenii, No. 3, May–June, 2012, pp. 411–413.

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Efanov, M.V., Galochkin, A.I. Phosphorylation of technical lignins. Chem Nat Compd 48, 457–459 (2012). https://doi.org/10.1007/s10600-012-0272-7

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  • DOI: https://doi.org/10.1007/s10600-012-0272-7

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