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Evaluation of Technological Parameters of Diabatic Rectification Column Operation with Various Schemes of Coolant Supply to Built-In Reflux Condensers on the Stages

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Chemical and Petroleum Engineering Aims and scope

A comparative analysis of several schemes of coolant supply to reflux condenser built into a multi-stage poppet diabatic rectification column was carried out. With changes in the coolant supply scheme the thermal characteristics of the column change, which affects the separation efficiency. The conducted studies show that the most advantageous scheme for supplying coolant to the built-in reflux condenser on the stages is a parallel one, which, in addition, allows regulation of coolant flow in each stage of the diabatic rectification column. It is shown that the main resistance to heat transfer (more than 74.2% for all the studied coolant supply schemes) is concentrated in heat transfer from the liquid condensing on the outer surface of the reflux condenser pipes.

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References

  1. A. A. Kiss, “Distillation technology − still young and full of breakthrough opportunities,” J. Chem. Technol. Biotechnol., 89, 479–498 (2014).

    Article  CAS  Google Scholar 

  2. R. Rivero, M. Garcia, and J. Urquiza, “Simulation, exergy analysis and application of diabatic distillation to a tertiary amyl methyl ether production unit of a crude oil refinery,” Energy, 29, No. 3, 467–489 (2004).

    Article  CAS  Google Scholar 

  3. N. A. Voinov, D. A. Zemtsov, N. V. Deryagina, et al., “A study of diabatic distillation in a column with a low pressure drop,” Chemical Engineering Research and Design, 185, 1–13 (2022).

    Article  CAS  Google Scholar 

  4. G. N. Mello, R. Battisti, N. S. Urruth, et al., “New distributed-action control strategy with simultaneous heating and cooling in trays of a pilot-scale diabatic distillation column,” Chemical Engineering Research and Design, 159, 424–438 (2020).

    Article  CAS  Google Scholar 

  5. V. K. Viktorov and A. Yu. Malyutin, “Method of synthesis of chemical engineering heat-integrated systems of rectification columns,” Izv. SPbGTI (TU), No. 14 (40), 97–101 (2012).

  6. M. К. Zakharov, Yu. A. Pisarenko., and O. I. Sycheva, “Comparison of methods of energy saving in liquid mixture rectification,” Izv. Vuz. Khim. Khim. Tekhnol., 64, No. 1, 85–92 (2021).

  7. M. Marin-Gallego, B. Mizzi, D. Rouzineau, et al., “Concentric heat integrated distillation column (HIDiC): a new specific packing design, characterization and pre-industrial pilot unit validation,” Chemical Engineering and Processing, 171, No. 5, 108643 (2022).

    Google Scholar 

  8. Y. H. Kim, “Energy saving of benzene separation process for environmentally friendly gasoline using an extended DWC (divided wall column),” Energy, 100, 58–65 (2016).

    Article  CAS  Google Scholar 

  9. J. D. Seader and S. C. Baer, Continuous Distillation Apparatus and Method, Final Report of University of Utah. Salt Lake City (US), 1984.

    Google Scholar 

  10. I. N. Madyshev, O. S. Dmitrieva, A. O. Myasova, and A. N. Nikolaev, “Determination of heat flows in built-in column reflux condenser during diabatic rectification,” Khim. Neftgaz. Mashinostr., No. 7, 3–6 (2022).

  11. E. D. Umrikhin and E. N. Konstantinov, “Influence of thermal effects on separation process in alcohol column,” Izv. Vuz., Pishch. Tekhnol., No. 1, 61–65 (2000).

  12. I. N. Madyshev, V. V. Kharkov, O. S. Dmitrieva, and V. E. Zinurov, “Energy saving in distillation by combining vortex contact device and thermal effects,” Therm. Sci. Eng. Prog., 34, 101431 (2022).

    Article  CAS  Google Scholar 

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Correspondence to I. N. Madyshev.

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Translated from Khimicheskoe i Neftegazovoe Mashinostroenie, Vol. 58, No. 10, pp. 6−10, October, 2022.

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Madyshev, I.N., Dmitrieva, O.S., Mayasova, A.O. et al. Evaluation of Technological Parameters of Diabatic Rectification Column Operation with Various Schemes of Coolant Supply to Built-In Reflux Condensers on the Stages. Chem Petrol Eng 58, 814–821 (2023). https://doi.org/10.1007/s10556-023-01167-8

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