Abstract
The effect of high temperature on the interface microstructure and interfacial shear strength of the continuous SiC fiber reinforced AlFe5Si2 matrix (45 vol.% SiCf/AlFe5Si2) composite was investigated. The composite was prepared by hot isostatic pressing (HIP), and then thermally exposed at 260/300/350/400/450 °C for 20/50/100 h, respectively. The interfacial shear strength of the composite with and without thermal exposure was measured by push-out test. The interface microstructure and phase compositions of the composite with and without thermal exposure were characterized by scanning electron microscopy, transmission electron microscopy and X-ray diffraction. Results showed that the interfacial reaction took place at the interface between SiC fiber and aluminum matrix and formed Al4C3 phase during the preparation process. The activation energy of Al4C3 growth at the C/Al interface was about 163 kJ/mol. With increasing the thermal exposure temperature and time, the interfacial shear strength of the composite declined, especially at temperatures above 400 °C. The brittle Al3.21SiO0.47 compound formed at temperatures above 400 °C mainly resulted in the severe strength deterioration of the interfacial reaction zone.
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References
Yu, K., Dollhopf, V., Kochendorfer, R.: CVD SiC/Al composites produced by a vacuum suction casting process. Compos. Sci. Technol. 46(1), 1–6 (1993)
Guo, Z.X., Derby, B.: Solid-state fabrication and interfaces of fibre reinforced metal matrix composites. Prog. Mater. Sci. 39(4–5), 411–495 (1995)
Pan, J., Yang, D.M., Yin, X.F., Fukunaga, H.: A study of the ultrasonic technique applied in fabrication of SiC fiber-reinforced aluminum composites. J. Mater. Res. 10(3), 596–601 (1995)
Iseki, T., Kameda, T., Maruyama, T.: Interfacial reactions between SiC and aluminium during joining. J. Mater. Sci. 19(5), 1692–1698 (1984)
Ochiai, S., Osamura, K.: Tensile strength of fibre-reinforced metal matrix composites with non-uniform fibre spacing. J. Mater. Sci. 24(10), 3536–3540 (1989)
Liu, H., Madaleno, U., Shinoda, T., Mishima, Y., Suzuki, T.: Interfacial reaction and strength of SiC fibres coated with aluminium alloys. J. Mater. Sci. 25(10), 4247–4254 (1990)
Clyne, T., Watson, M.: Interfacial mechanics in fiber-reinforced metals. Compos. Sci. Technol. 42(1–3), 25–55 (1991)
Watson, M.C., Clyne, T.W.: The use of single fiber pushout testing to explore interfacial mechanics in SiC monofilament-reinforced Ti―II. Application of the test to composite material. Acta. Metall. Mater. 40(1), 141–148 (1992)
Tripathi, D., Turton, T., Chen, F., Jones, F.R.: A new method to normalize the effect of matrix properties on the value of interfacial shear strength obtained from the fragmentation test. J. Mater. Sci. 32(18), 4759–4765 (1997)
Zeng, W.D., Peters, P.W.M., Tanaka, Y.: Interfacial bond strength and fracture energy at room and elevated temperature in titanium matrix composites (SCS-6/Timetal 834). Compos. Part A. 33(9), 1159–1170 (2002)
Chen, L.G., Lin, S.J.: Effect of nickel coating on the interfacial shear strengths of SiC fiber reinforced 7075 aluminum composites. J. Electrochem. Soc. 149, C383–C389 (2002)
Drzal, L.T., Madhukar, M.: Fiber matrix adhesion and its relationship to composite mechanical-properties. J. Mater. Sci. 28(3), 569–610 (1993)
Juergens, M., da Silva, M.T.V.H.P.F., Heimbs, S., Lang, H., Ladstaetter, E., Hombergsmeier, E.: Pull-out testing of multiscale structured metallic z-reinforcements for CFRP laminates. Compos. Struct. 161, 384–392 (2017)
Kallas, M.N., Koss, D.A., Hahn, H.T., Hellmann, J.R.: Interfacial stress state present in a “thin-slice” fibre push-out test. J. Mater. Sci. 27(14), 3821–3826 (1992)
Chen, L.G., Lin, S.J., Chang, S.Y.: Analysis of interfacial shear strength of SiC fiber reinforced 7075 aluminum composite by pushout microindentation. Metall. Mater. Trans. A. 36A(7), 1937–1945 (2005)
Jiang, Y.Q., Liu, J.H., Wu, X.B.: A measure of interfacial frictional shear strength of MMC. Chin. J. Mater. Res. 8(4), 378–380 (1994)
Yang, C.J., Jeng, S.M., Yang, J.-M.: Interfacial properties measurement for SiC fiber-reinforced titantum alloy composites. Scripta. Metall. Mater. 24(3), 469–474 (1990)
Ningal, X.J., Pirouzal, P.: The microstructure of SCS-6 SiC fiber. J. Mater. Res. 6(10), 2234–2248 (1991)
Lu, X., Yang, Y., Ma, Z., Liu, C., Chen, Y., Al, Y.: Kinetics and mechanism of interfacial reaction in SCS-6SiC continuous fiber-reinforced Ti-Al intermetallic matrix composites. T. Nonferr. Metal. Soc. 16(1), 77–83 (2006)
Guo, Z.X., Derby, B.: Interfaces in Ti3Al composites reinforced with sigma SiC fiber. Scripta. Metall. Mater. 30(1), 89–94 (1994)
Breuer, J., Wilger, T., Friesel, M., Herzig, C.: Interstitial and substitutional diffusion of metallic solutes in Ti3Al. Intermetallics. 7(3–4), 381–388 (1999)
Yasutomi, Y., Sawada, J., Kikuchi, T., Nakamura, K., Manabe, Y., Nagano, K., Kuroda, H., Sumi, T., Kubokawa, H., Nagai, M., Kogure, H., Sawai, Y., Kishi, T.: Effects of the SiC/Al interface reaction on fracture behavior of a composite conductor using SiC fiber reinforced aluminum for next generation power equipment. J. Mater. Sci. 34(7), 1583–1593 (1999)
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The authors gratefully acknowledge the financial support of the National Natural Science Foundation of China, grant number U1537212, 51471019 and the National Key Research and Development Program of China, grant number 2016YFB0300901.
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Chu, D., Ma, Y., Tang, P. et al. Effect of Thermal Exposure on the Interface Microstructure and Interfacial Shear Strength of the SiC Fiber Reinforced AlFe5Si2 Matrix Composite. Appl Compos Mater 27, 95–105 (2020). https://doi.org/10.1007/s10443-020-09798-3
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DOI: https://doi.org/10.1007/s10443-020-09798-3