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Simultaneous Determination of Organic Acids, Inorganic Anions, and Alditols in Wine with Valve-Switching Ion Chromatography

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Abstract

A valve-switching ion chromatography method coupled with conductivity and pulsed amperometric detection has been set up for the simultaneous determination of organic acids, inorganic anions and alditols in wine. The system, based on valve-switching technique, consisted of two pumps, two analytical columns and a trap column connected in series via one six-port valve. In addition, the optimal valve-switching time and chromatographic conditions were explored to obtain a good linearity, precision, accuracy, and sensitivity with a mean correlation coefficient of > 0.99, repeatability of 0.62–6.18% for eight replicates, and the average spiked recovery of 96.66%. The new method was successfully applied in the analysis of six kinds of wine from different regions.

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Acknowledgements

This research was supported by the National Natural Science Foundation of China (Nos. 21405166, U1507203) and the National Public Welfare Special Fund for “Food Chemical Risk Substances Screening and Warning Demonstration Research” (No. 2012424012).

Funding

This study was funded by the National Natural Science Foundation of China (Nos. 21405166, U1507203) and the National Public Welfare Special Fund for “Food Chemical Risk Substances Screening and Warning Demonstration Research” (No. 2012424012).

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Author notes

  1. Fangfang Li and Yan Bao contributed equally to this study and share first authorship.

Authors and Affiliations

  1. Public Laboratory, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, No. 189 Songling Road, Qingdao, 266101, China

    Fangfang Li, Yan Bao, Yun Fa & Huizhou Liu

  2. School of Materials Science and Engineering, Qingdao University of Science and Technology, No. 53 Zhengzhou Road, Qingdao, 266000, China

    Yuexue Yu

  3. Technical Center of Shandong Entry-Exit Inspection and Quarantine Bureau, No. 70 Qutangxia Road, Qingdao, 266002, China

    He Cui

  4. University of Chinese Academy of Science, Beijing, 100049, China

    Yun Fa & Huizhou Liu

Authors
  1. Fangfang Li
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  2. Yan Bao
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  3. Yuexue Yu
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  4. He Cui
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  5. Yun Fa
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  6. Huizhou Liu
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Correspondence to Yun Fa or Huizhou Liu.

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This article does not contain any studies with human participants performed by any of the authors.

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Li, F., Bao, Y., Yu, Y. et al. Simultaneous Determination of Organic Acids, Inorganic Anions, and Alditols in Wine with Valve-Switching Ion Chromatography. Chromatographia 81, 1103–1108 (2018). https://doi.org/10.1007/s10337-018-3563-8

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  • DOI: https://doi.org/10.1007/s10337-018-3563-8

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