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Erratum to: J Solid State Electrochem (2013) 17:79–97
DOI 10.1007/s10008-012-1834-0
The authors regret errors in the experimental part (description of the synthesis of 1-methyl-1′-trimethoxypropylsilane[4,4′]bipyridinium diiodide, compound 2):
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1.
After separation of the fine precipitate by centrifugation, the raw product is washed twice. The correct volume of toluene for each washing step should be rather 45 ml than 4 ml. Use of the incorrect amount of toluene may result in a contaminated product.
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2.
The interpretation of the 13C-NMR signals at 148.13 and 148.46 ppm as ‘CH’ is misleading. The respective carbon atoms are quarternary.
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The online version of the original article can be found at http://dx.doi.org/10.1007/s10008-012-1834-0.
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Ruff, A., Schuler, P. & Speiser, B. Erratum to: Redox-active silica nanoparticles. Part 6. Synthesis and spectroscopic and electrochemical characterization of viologen-modified Stöber silica particles with diameters of approximately 125 nm. J Solid State Electrochem 17, 1787 (2013). https://doi.org/10.1007/s10008-013-2058-7
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DOI: https://doi.org/10.1007/s10008-013-2058-7