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One-pot synthesis of highly dispersed palladium nanoparticles on acetylenic ionic liquid polymer functionalized carbon nanotubes for electrocatalytic oxidation of glucose

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Abstract

A facile method for one-pot synthesis of highly dispersed palladium nanoparticles on acetylenic ionic liquid polymer functionalized carbon nanotubes (PdNPs-AILP-CNTs) has been developed in this paper. The nanohybrids are prepared by polymerization of acetylenic ionic liquid monomers catalyzed by PdCl2, which is further reduced to PdNPs by NaBH4 on CNTs in one pot and characterized by Fourier transform infrared spectroscopy, Raman spectroscopy, thermogravimetric analysis, and transmission electron microscopy. The electrocatalytic oxidation of glucose on the PdNPs-AILP-CNT nanohybrids is also investigated by cyclic voltammetry and chronoamperometry. The results show that the PdNPs with a particle size of around 3.5 nm disperse uniformly on CNTs, and PdNPs-AILP-CNT nanohybrids have good electrocatalytic performance for glucose oxidation.

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Acknowledgments

This work is supported by the NSFC (20975033, 20905024), the Program for Changjiang Scholars and Innovative Research Team in University (PCSIRT), and the National Basic Research Program of China (no. 2009CB421601).

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Authors and Affiliations

  1. State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University, Changsha, 410082, People’s Republic of China

    Yinjie Kuang, Bohua Wu, Dan Hu, Xiaohua Zhang & Jinhua Chen

  2. School of Chemistry and Biology Engineering, Changsha University of Science & Technology, Changsha, 410114, People’s Republic of China

    Yinjie Kuang

Authors
  1. Yinjie Kuang
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  2. Bohua Wu
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  3. Dan Hu
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  4. Xiaohua Zhang
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  5. Jinhua Chen
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Corresponding author

Correspondence to Jinhua Chen.

Electronic supplementary materials

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Fig. S1

1H NMR spectra of the [MPYI]Br (DOC 1381 kb)

Fig. S2

ESI mass spectrum the [MPYI]Br (DOC 1120 kb)

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Kuang, Y., Wu, B., Hu, D. et al. One-pot synthesis of highly dispersed palladium nanoparticles on acetylenic ionic liquid polymer functionalized carbon nanotubes for electrocatalytic oxidation of glucose. J Solid State Electrochem 16, 759–766 (2012). https://doi.org/10.1007/s10008-011-1430-8

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  • DOI: https://doi.org/10.1007/s10008-011-1430-8

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