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Bonding of composite resins to PEEK: the influence of adhesive systems and air-abrasion parameters

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Abstract

Objective

The objective of the study was to investigate the tensile bond strength (TBS) to polyaryletheretherketone (PEEK) after different pretreatment and conditioning methods.

Methods

Four hundred PEEK specimens were fabricated and allocated to the following air-abrasion methods (n 1 = 80/pretreatment): (i) 50 μm Al2O3 (0.05 MPa); (ii) 50 μm Al2O3 (0.35 MPa); (iii) 110 μm Al2O3 (0.05 MPa); (iv) 110 μm Al2O3 (0.35 MPa); and (v) Rocatec 110 μm (0.28 MPa). These pretreatments were combined with the following conditioning methods (n 2 = 20/pretreatment/conditioning): (a) visio.link (VL); (b) Monobond Plus/Heliobond (MH); (c) Scotchbond Universal (SU); and (d) dialog bonding fluid (DB). After veneering of all specimens with dialog occlusal and aging (28 days H2O, 37 °C + 20,000 thermal cycles, 5/55 °C), TBS was measured. Data was analysed using Kaplan–Meier survival analysis with Breslow–Gehan test and Cox-regressions.

Results

The major impact on TBS showed the conditioning, followed by the air-abrasion-pressure, while the grain size of the air-abrasion powder did not show any effect. Specimens air-abraded at 0.35 MPa showed the highest survival rates. However, within VL groups, this observation was not statistically significant. Within MH groups, pretreatment using 110 μm Al2O3 and 0.05 MPa resulted in higher survival rates compared to groups treated with 50 and 110 μm Al2O3 using a pressure of 0.35 MPa. The use of VL showed the highest survival rates between the adhesive systems and the TBS values higher than 25 MPa independent of the pretreatment method. As an exception, only VL showed significantly higher survival rates when compared to MH.

Conclusions

The adequate choice of the adhesive system and higher pressures improved the TBS between PEEK and veneering resin composite. The particle size had no major impact.

Clinical relevance

According to this study, best veneering of PEEK with dialog occlusal can be achieved by conditioning with visio.link in combination with the pretreatment of airborne particle abrasion at a pressure of 0.35 MPa.

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Acknowledgments

The authors would like to thank Schütz Dental, bredent, and Ivoclar Vivadent for material support of this study.

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Correspondence to Bogna Stawarczyk.

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All procedures performed in studies involving human participants are in accordance with the ethical standards of the institutional and/or national research committee and with the 1964 Helsinki Declaration and its later amendments or comparable ethical standards.

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The authors declare that they have no conflict of interest.

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This study received no funding.

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This article does not contain any studies with human participants or animals performed by any of the authors.

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For this type of study, formal consent is not required.

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Stawarczyk, B., Taufall, S., Roos, M. et al. Bonding of composite resins to PEEK: the influence of adhesive systems and air-abrasion parameters. Clin Oral Invest 22, 763–771 (2018). https://doi.org/10.1007/s00784-017-2151-x

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  • DOI: https://doi.org/10.1007/s00784-017-2151-x

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