Clinical Oral Investigations

, Volume 14, Issue 2, pp 187–192 | Cite as

In vitro comparative bond strength of contemporary self-adhesive resin cements to zirconium oxide ceramic with and without air-particle abrasion

  • Markus B. Blatz
  • Jin-Ho Phark
  • Fusun Ozer
  • Francis K. Mante
  • Najeed Saleh
  • Michael Bergler
  • Avishai Sadan
Original Article

Abstract

This study compared shear bond strengths of six self-adhesive resin cements to zirconium oxide ceramic with and without air-particle abrasion. One hundred twenty zirconia samples were air-abraded (group SB; n = 60) or left untreated (group NO). Composite cylinders were bonded to the zirconia samples with either BisCem (BC), Maxcem (MC), G-Cem (GC), RelyX Unicem Clicker (RUC), RelyX Unicem Applicator (RUA), or Clearfil SA Cement (CSA). Shear bond strength was tested after thermocycling, and data were analyzed with analysis of variance and Holm–Sidak pairwise comparisons. Without abrasion, RUA (8.0 MPa), GC (7.9 MPa), and CSA (7.6 MPa) revealed significantly higher bond strengths than the other cements. Air-particle abrasion increased bond strengths for all test cements (p < 0.001). GC (22.4 MPa) and CSA (18.4 MPa) revealed the highest bond strengths in group SB. Bond strengths of self-adhesive resin cements to zirconia were increased by air-particle abrasion. Cements containing adhesive monomers (MDP/4-META) were superior to other compositions.

Keywords

Zirconia ceramic Air abrasion Self-adhesive cements Bond strength 

References

  1. 1.
    Aboushelib MN, Kleverlaan CJ, Feilzer AJ (2007) Selective infiltration-etching technique for a strong and durable bond of resin cements to zirconia based materials. J Prosthet Dent 98:379–388CrossRefPubMedGoogle Scholar
  2. 2.
    Aboushelib MN, Matinlinna JP, Salameh Z, Ounsi H (2008) Innovations in bonding to zirconia-based materials: Part I. Dent Mater 24:1268–1272CrossRefPubMedGoogle Scholar
  3. 3.
    Atsu SS, Kilicarslan MA, Kucukesmen HC, Aka PS (2006) Effect of zirconium-oxide ceramic surface treatments on the bond strength to adhesive resins. J Prosthet Dent 95:430–436CrossRefPubMedGoogle Scholar
  4. 4.
    Blatz MB, Sadan A, Kern M (2003) Resin-ceramic bonding—a review of the literature. J Prosthet Dent 89:268–274CrossRefPubMedGoogle Scholar
  5. 5.
    Blatz MB, Sadan A, Maltezos C, Blatz U, Mercante D, Burgess JO (2004) In-vitro durability of the resin bond to feldspathic ceramics. Am J Dent 17:169–172PubMedGoogle Scholar
  6. 6.
    Blatz MB, Sadan A, Martin J, Lang B (2004) In vitro evaluation of shear bond strengths of resin to densely-sintered high-purity zirconium oxide ceramic after long-term storage and thermal cycling. J Prosthet Dent 91:356–362CrossRefPubMedGoogle Scholar
  7. 7.
    Blatz MB, Chiche G, Holst S, Sadan A (2007) Influence of surface treatment and simulated aging on bond strengths of luting agents to zirconia. Quintessence Int 38:745–753PubMedGoogle Scholar
  8. 8.
    Blatz MB, Oppes S, Chiche G, Holst S, Sadan A (2008) Influence of cementation technique on fracture strength and leakage of alumina all-ceramic crowns after cyclic loading. Quintessence Int 39:23–32PubMedGoogle Scholar
  9. 9.
    Della Bona A, Donassollo TA, Demarco FF, Barrett AA, Mecholsky JJ (2007) Characterization and surface treatment effects on topography of a glass-infiltrated alumina/zirconia-reinforced ceramic. Dent Mater 23:769–775CrossRefPubMedGoogle Scholar
  10. 10.
    Denry I, Kelly JR (2008) State of the art of zirconia for dental applications. Dent Mater 24:299–307CrossRefPubMedGoogle Scholar
  11. 11.
    Derand P, Derand T (2000) Bond strength of luting cements to zirconium oxide ceramics. Int J Prosthodont 13:131–135PubMedGoogle Scholar
  12. 12.
    Hill EE (2007) Dental Cements for definitive luting: a review and practical clinical considerations. Dent Clin N Am 643-658Google Scholar
  13. 13.
    Kern M, Thompson VP (1995) Bonding to glass infiltrated alumina ceramic: adhesive methods and their durability. J Prosthet Dent 73:240–249CrossRefPubMedGoogle Scholar
  14. 14.
    Kern M, Wegner SM (1998) Bonding to zirconia ceramic: adhesion methods and durability. Dent Mater 14:64–71CrossRefPubMedGoogle Scholar
  15. 15.
    Kumbuloglu O, Lassila LVJ, User A, Vallittu PK (2006) Bonding of resin composite luting cements to zirconium oxide by two air-particle abrasion methods. Oper Dent 31–2:248–255CrossRefGoogle Scholar
  16. 16.
    Leung Y, Morris MD (1995) Characterization of the chemical interactions between 4-META and enamel by Raman spectroscopy. Dent Mater 11:191–195CrossRefPubMedGoogle Scholar
  17. 17.
    Lohbauer U, Zipperle M, Rischka K, Petschelt A, Muller FA (2008) Hydroxylation of dental zirconia surfaces: characterization and bonding potential. J Biomed Mater Res Part B: Appl Biomater 87B:461–467CrossRefGoogle Scholar
  18. 18.
    Lüthy H, Loeffel O, Hammerle CHF (2006) Effect of thermocycling on bond stregth of luting cements to zirconia ceramic. Dent Mater 22:195–200CrossRefPubMedGoogle Scholar
  19. 19.
    Mitra SB (2009) Dental Cements: formulations and handling techniques. In: Curtis RV, Watso F (eds) Dental biomaterials; imaging, testing and modelling, 2nd edn. Woodhead publishing limited, Cambridge, pp 162–193Google Scholar
  20. 20.
    Ozcan M, Alkumru HN, Gemalmaz D (2001) The effect of surface treatment on the shear bond strength of luting cement to a glass-infiltrated alumina ceramic. Int J Prosthodont 14:335–339PubMedGoogle Scholar
  21. 21.
    Ozcan M, Vallittu PK (2003) Effect of surface conditioning methods on the bond strength of luting cement to ceramics. Dent Mater 19:725–731CrossRefPubMedGoogle Scholar
  22. 22.
    Palacios RP, Johnson GH, Phillips KM, Raigrodski AJ (2006) Retention of zirconium oxide crowns with three types of cements. J Prosthet Dent 96:104–114CrossRefPubMedGoogle Scholar
  23. 23.
    Piwowarczyk A, Lauer HC (2003) Mechanical properties of luting cements after water storage. Oper Dent 28:535–542PubMedGoogle Scholar
  24. 24.
    Piwowarczyk A, Lauer HC, Sorensen JA (2004) In vitro shear bond strength of cementing agents to fixed prosthodontic restorative materials. J Prosthet Dent 92:265–273CrossRefPubMedGoogle Scholar
  25. 25.
    Quaas AC, Yang B, Kern M (2007) Panavia F 2.0 bonding to contaminated zirconia ceramic after different cleaning procedures. Dent Mater 23:506–512CrossRefPubMedGoogle Scholar
  26. 26.
    Radovic I, Monticelli F, Goracci C, Vulicevic ZR, Ferrari M (2008) Self-adhesive cements: a literature review. 10:251–258Google Scholar
  27. 27.
    Wolfart M, Lehmen F, Wolfart S, Kern M (2007) Durability of the resin bond strength to zirconia ceramic after using different surface conditioning methods. Dent Mater 23:45–50CrossRefPubMedGoogle Scholar

Copyright information

© Springer-Verlag 2009

Authors and Affiliations

  • Markus B. Blatz
    • 1
  • Jin-Ho Phark
    • 2
  • Fusun Ozer
    • 1
  • Francis K. Mante
    • 1
  • Najeed Saleh
    • 1
  • Michael Bergler
    • 1
  • Avishai Sadan
    • 2
  1. 1.Department of Preventive and Restorative SciencesSchool of Dental Medicine, University of PennsylvaniaPhiladelphiaUSA
  2. 2.Department of Comprehensive CareSchool of Dental Medicine, Case Western Reserve UniversityClevelandUSA

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