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Application of boron-doped diamond electrode for rapid and sensitive voltammetric detection of vildagliptin in anionic surfactant medium

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Abstract

The electrochemical evaluation of vildagliptin in solutions with and without surfactant was investigated using square wave and cyclic voltammetry methods. For this purpose, anionic surfactant showed a positive effect on the anodic pretreated boron-doped diamond electrode surface. Vildagliptin gave an irreversible wave at approximately + 1.28 V at Britton–Robinson buffer (containing 0.5 mM SDS pH 11.0) medium. Using square wave voltammetry, the anodic current signal showed a linear correlation with concentrations ranging from 2.94 µM to 55.86 µM. The limit of detection of 77.52 nM and the relative standard deviation of 1.19% were estimated at a concentration level of 2.94 µM (n = 10). Without any separation, the new electroanalytical method was effectively employed to vildagliptin determination in pharmaceutical formulations and urine samples.

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Authors and Affiliations

  1. Department of Chemistry and Chemical Processing Technology, Technical Sciences Vocational School, Batman University, Batman, Turkey

    Yalçın Altunkaynak

  2. Department of Medical Services and Techniques, Health Services Vocational School, Batman University, Batman, Turkey

    Günay Önal

  3. Department of Chemistry, Faculty of Arts and Sciences, Batman University, Batman, Turkey

    Abdulkadir Levent

Authors
  1. Yalçın Altunkaynak
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  2. Günay Önal
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  3. Abdulkadir Levent
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Correspondence to Abdulkadir Levent.

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Altunkaynak, Y., Önal, G. & Levent, A. Application of boron-doped diamond electrode for rapid and sensitive voltammetric detection of vildagliptin in anionic surfactant medium. Monatsh Chem 154, 181–190 (2023). https://doi.org/10.1007/s00706-022-03020-9

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  • DOI: https://doi.org/10.1007/s00706-022-03020-9

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