Summary.
Solvent-free irradiation of thiomorpholides with two kinds of methylating agents under microwave or ultrasonic conditions gave the corresponding thioesters in high yield. The method is simple and avoids prolonged heating with solvents.
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Darabi, H., Aghapoor, K. & Tabar-Heidar, K. A Fast and Solvent-Free Conversion of Thioamides into Thioesters. Monatshefte für Chemie 135, 79–81 (2004). https://doi.org/10.1007/s00706-003-0087-0
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DOI: https://doi.org/10.1007/s00706-003-0087-0