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Semi-Micro Preparation and Characterization of Bonded Phase ODS-Silica Prepared from Rice Husk Silica

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Abstract.

Bonded phase ODS-silica has been prepared using purified silica prepared from rice husk by burning, reflux with sodium hydroxide solution and precipitation as a gel. The gel was spray dried, further purified by washing with concentrated hydrochloric acid then distilled water prior to vacuum drying and silanization and end-capping. The product’s physical and chromatographic properties are reported.

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Author information

Authors and Affiliations

  1. School of Chemistry, The Queen’s University of Belfast, BT9 5AG, Belfast, Northern Ireland, UK

    Duncan Thorburn Burns

  2. Department of Chemistry, King Mongkut’s Institute of Technology, 10520, Ladkrabang, Bangkok, Thailand

    Kanita Tungkananurak & Damrongsak Jadsadapattarakul

Authors
  1. Duncan Thorburn Burns
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  2. Kanita Tungkananurak
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  3. Damrongsak Jadsadapattarakul
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Corresponding author

Correspondence to Kanita Tungkananurak.

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Burns, D., Tungkananurak, K. & Jadsadapattarakul, D. Semi-Micro Preparation and Characterization of Bonded Phase ODS-Silica Prepared from Rice Husk Silica. Microchim Acta 154, 81–85 (2006). https://doi.org/10.1007/s00604-005-0474-9

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  • DOI: https://doi.org/10.1007/s00604-005-0474-9

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