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Study on the Chemistry and Structure of (Na(1−x)Bix)(Nb(1−y)Mny)O3 Ceramics by XPS, AES and EPMA

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Abstract.

The (Na1−xBix)(MnyNb1−y)O3 ceramics are new compounds, obtained for the first time, on the base of sodium niobate with substitution of bismuth manganite. It was shown that the solubility limit for Mn ions in sodium niobate lattice does not exceed 1% at. Therefore, the co-doping with Bi ions was proposed to increase this limit. Bismuth ions are expected to replace Na ions and to ensure charge compensation in the formed compound, thus enhancing possibility of accumulation of the Mn ions in solution without losing the appropriate electrical and optical properties. To study the morphology of produced ceramic four methods of sample characterization were used: X-ray photoelectron spectroscopy (XPS), Auger electron spectroscopy (AES), electron microprobe analysis (EPMA) and Scanning Electron Microscopy (SEM).

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Authors and Affiliations

  1. Polish Academy of Sciences, Institute of Physics, Al. Lotników 32/46, PL-02668, Warsaw, Poland

    Krystyna Ławniczak-Jabłońska, Iraida N. Demchenko, Edyta Piskorska & Jakub Kachniarz

  2. University of Silesia, Institute of Physics, ul. Uniwersytecka 4, PL-40007, Katowice, Poland

    Andrzej Molak

  3. Department of Applied Physics, University of Turku, Vesilinnantie 5, FI-20014, Turku, Finland

    Markku Heinonen

Authors
  1. Krystyna Ławniczak-Jabłońska
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  2. Iraida N. Demchenko
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  3. Edyta Piskorska
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  4. Andrzej Molak
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  5. Jakub Kachniarz
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  6. Markku Heinonen
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Corresponding author

Correspondence to Krystyna Ławniczak-Jabłońska.

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Ławniczak-Jabłońska, K., Demchenko, I., Piskorska, E. et al. Study on the Chemistry and Structure of (Na(1−x)Bix)(Nb(1−y)Mny)O3 Ceramics by XPS, AES and EPMA. Microchim. Acta 145, 95–99 (2004). https://doi.org/10.1007/s00604-003-0136-8

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  • DOI: https://doi.org/10.1007/s00604-003-0136-8

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