Abstract
Samples of akaganeite (β-FeOOH) and goethite (α-FeOOH) have been studied after heating at various temperatures up to 800 °C. X-ray diffraction and Mössbauer spectroscopy measurements showed that slightly below the temperatures at which the samples transform to hematite (α-Fe2O3) the oxyhydroxide phases become nanocrystalline.
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References
Brown, G. (1980) Associated Minerals in Crystal Structures of Clay Minerals and Their X-ray Identification Mineralogical Society Monograph no. 5, pp. 361–410. London: Mineralogical Society
Paterson, E., Tait, J.: Clay Minerals 12, 245 (1977)
Koch, C.J.W., Madsen, M.B., Mørup S.: Hyperfine Interact. 28, 549 (1986)
Klug, H.P., Alexander, L.E.: X-ray Diffraction Procedures for Polycrystalline and Amorphous Materials, 966 pp. New York: Wiley 1974 5. Chambaere, D.G., De Grave, E.: J. Magn. Magn. Mater. 44, 349 (1984)
Mørup, S., Madsen, M.B., Franck, J., Villadsen, J., Koch, C.J.W.: J. Magn. Magn. Mater. 40, 163 (1983)
Mørup, S., Bødker, F., Hendriksen, P.V., Linderoth, S.: Phys. Rev. B 52, 287 (1995)