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Preparation and characterization of the crystalline inclusion complexes of α- and γ-cyclodextrins with poly(butylene carbonate)

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Abstract.

Poly(butylene carbonate) was found to form crystalline inclusion complexes with α-cyclodextrin and γ-cyclodextrin, but it did not form crystalline inclusion complex with β-cyclodextrin. The crystalline inclusion complexes are also called pseudopolyrotaxanes. Thermogravimetric analysis, FTIR spectroscopy, X-ray diffraction, 1H NMR spectroscopy, 2D NOESY NMR spectroscopy and 13C cross-polarization magic-angle-spinning NMR spectroscopy were used to characterize the structures and properties of those crystalline inclusion complexes.

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Authors and Affiliations

  1. School of Chemistry and Chemical Technology, Shanghai Jiao Tong University, Shanghai 200240, China, , , , ,

    Jingye Li, Yiyong Mai & Deyue Yan

  2. Analytical Center and the Key Laboratory of Education Ministry for Optical and Magnetic Resonance Spectroscopy, East China Normal University, Shanghai 200062, China, , , , ,

    Qun Chen

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  1. Jingye Li
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  2. Yiyong Mai
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  3. Deyue Yan
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  4. Qun Chen
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Li, J., Mai, Y., Yan, D. et al. Preparation and characterization of the crystalline inclusion complexes of α- and γ-cyclodextrins with poly(butylene carbonate). Colloid Polym Sci 281, 267–274 (2003). https://doi.org/10.1007/s00396-002-0770-4

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  • DOI: https://doi.org/10.1007/s00396-002-0770-4

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