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Two-color thermosensors based on [Y\(_{1-x}\)Dy\(_x\)(acetylacetonate)\(_3\)(1,10-phenanthroline)] molecular crystals

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Abstract

We develop a two-color thermometry (TCT) phosphor based on [Y\(_{1-x}\)Dy\(_x\)(acetylacetonate)\(_3\)(1,10-phenanthroline)] ([Y\(_{1-x}\)Dy\(_x\)(acac)\(_3\)(phen)]) molecular crystals for use in heterogeneous materials. We characterize the optical properties of [Y\(_{1-x}\)Dy\(_x\)(acac)\(_3\)(phen)] crystals at different temperatures and Dy concentrations, and find that the emission is strongly quenched by increasing temperature and concentration. We also observe a broad background emission (due to the ligands) and find that [Y\(_{1-x}\)Dy\(_x\)(acac)\(_3\)(phen)] photodegrades under 355 nm illumination with the photodegradation resulting in decreased luminescence intensity. However, while decreasing the overall emission intensity, photodegradation is not found to influence the integrated intensity ratio of the \({}^4I_{15/2} \rightarrow {}^6H_{15/2}\) and \({}^4F_{9/2} \rightarrow {}^6H_{15/2}\) transitions. This ratio allows us to compute the temperature of the complex. Based on the temperature dependence of these ratios; we calculate that [Y\(_{1-x}\)Dy\(_x\)(acac)\(_3\)(phen)] has a maximum sensitivity of 1.5% K\(^{-1}\) and our TCT system has a minimum temperature resolution of 1.8 K. Finally, we demonstrate the use of [Y\(_{1-x}\)Dy\(_x\)(acac)\(_3\)(phen)] as a TCT phosphor by determining a dynamic temperature profile using the emission from [Y\(_{1-x}\)Dy\(_x\)(acac)\(_3\)(phen)].

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Acknowledgements

This work was supported by the Air Force Office of Scientific Research, Award # FA9550-15-1-0309 to Washington State University.

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  1. Applied Sciences Laboratory, Institute for Shock Physics, Washington State University, Spokane, WA, 99210-1495, USA

    Benjamin R. Anderson, Ray Gunawidjaja & Hergen Eilers

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Anderson, B.R., Gunawidjaja, R. & Eilers, H. Two-color thermosensors based on [Y\(_{1-x}\)Dy\(_x\)(acetylacetonate)\(_3\)(1,10-phenanthroline)] molecular crystals. Appl. Phys. B 123, 62 (2017). https://doi.org/10.1007/s00340-017-6638-6

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