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Synthesis and thermal properties of new polyester based on indane-1,3-diol and terephtaloyl chloride

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SUMMARY

New aromatic polyester was synthetized by polycondensation of indane-1,3-diol and terephthaloyl chloride. The indane-1,3-diol was synthesised by metal hydride reduction and characterized by IR, 1H and 13C NMR. Two polycondensation methods was used : solution and interfacial polycondensation in presence of various quaternary ammonium salts. The obtained polymers were characterized by differential scanning calorimetry (DSC) and viscosities measurements. All polymers had glass transition temperature (Tg) in the range of 72–77°C and melting temperature (Tm) in the range of 152–184°C.

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Authors and Affiliations

  1. Institut de Chimie, Université des Sciences et de la Technologie Houari Boumediene, Bp 32 El-alia, 16111 Bab-ezzouar Alger, Algerie, , , , , , XX

    H. Guemmour & A. Benaboura

  2. Laboratoire de Chimie Macromoléculaire, Université Pierre et Marie Curie, Tour 44, 1ier étage, 4 place Jussieu, 75252 Paris Cedex 05, France, , , , , , FR

    F. Carrière

Authors
  1. H. Guemmour
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  2. F. Carrière
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  3. A. Benaboura
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Received: 19 July 2000/Revised version: 10 December 2000/Accepted: 3 January 2001

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Guemmour, H., Carrière, F. & Benaboura, A. Synthesis and thermal properties of new polyester based on indane-1,3-diol and terephtaloyl chloride. Polymer Bulletin 46, 1–6 (2001). https://doi.org/10.1007/s002890170081

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  • DOI: https://doi.org/10.1007/s002890170081

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