Skip to main content
SpringerLink
Log in

Synthesis of polyorganosiloxane particles

  • Published:
Polymer Bulletin Aims and scope Submit manuscript

Summary

Hybrid particles have been synthesized from methyltriethoxysilane (METOS) by the sol-gel process. The particle size, size distribution, particle surface morphology conductivity and pH of the reaction solution at different reaction times were determined. Compared with tetraethyl orthosilicate (TEOS) and p-(chloromethyl)phenyl-trimethoxysilane (CMPTOS), MTEOS has a slower hydrolysis rate.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Philipse A. P. and Vrij A. (1989) J. Colloid and Interface Science 128(1): 121

    Article  CAS  Google Scholar 

  2. Ramamurthi S. D., Xu Z and Payne D. A (1990) J. Am. Chem. Soc. 73(9): 2760

    CAS  Google Scholar 

  3. Chant J. M., Bleay S. M., Harris B., Russell-Floyd R., Cooke R. G. and Scott V. D. (1995) J. Mat. Sci. 30: 2769

    Article  CAS  Google Scholar 

  4. Schmidt H. (1994) J. Sol-gel Sci and Tech. 1: 217

    Article  CAS  Google Scholar 

  5. Brinker C. J. and Scherer G. W.,(1990) Sol-Gel Science, Academic Press

  6. Wei Y., Jin D., Yang C. and Wei G. (1996) ACS Polymer Materia Sciences and Engineering, 74:244

    CAS  Google Scholar 

  7. Ellsworth M. W. and Novak B.M. (1991) J. Am. Chem. Soc. 113: 2756

    Article  CAS  Google Scholar 

  8. Tewari P. H., Hunt A. J. And Loffus K. D, (1985) Mater. Lett. 3:363

    Article  CAS  Google Scholar 

  9. Chujo Y., Ihara E., Kure S. And Sausa T. (1993) Macromolecules 26: 5681

    Article  CAS  Google Scholar 

  10. Iler R. K. (1979) The Chemistry of Silica, Wiley New York,

    Google Scholar 

  11. Stöber W., Fink A., and Bohn E., (1968) J. Colloid and Interface Sci. 26: 62

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Chemistry, Virginia Commonwealth University, 23284, Richmond, VA, USA

    Rui Yin & Raphael M. Ottenbrite

  2. Bermuda Hundred, ICI Film, 23860, Hopewell, VA, USA

    Junaid A. Siddiqui

Authors
  1. Rui Yin
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Raphael M. Ottenbrite
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Junaid A. Siddiqui
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Yin, R., Ottenbrite, R.M. & Siddiqui, J.A. Synthesis of polyorganosiloxane particles. Polymer Bulletin 38, 23–25 (1997). https://doi.org/10.1007/s002890050014

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s002890050014

Keywords

Search

Navigation