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Polyimides with 3,3’-Bipyrrolidine-2,2’,5,5’-Tetrone Units

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Summary

New linear polymers with 3,3’-bipyrrolidine-2,2’,5,5’-tetrone units were prepared by the ring-coupling reaction of α,α’-bis(chlorosuccinimide)s under the action of dust zinc and iodine. Bis(α-chlorosuccinimide)s were synthesized by the dehydrocyclization of the bismaleamic acids in the presence of thionyl chloride. The IR, 1H-NMR and 13C-NMR spectroscopy and elemental analysis confirmed the structure of monomers and polymers. The thermal behaviour of the polymers was monitored using dynamic thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC).

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Authors and Affiliations

  1. Institute of Macromolecular Chemistry “Petru Poni”, 41A Gr. Ghica Voda Alley, Iasi, Romania

    Constantin Gaina & Viorica Gaina

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  1. Constantin Gaina
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  2. Viorica Gaina
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Correspondence to Constantin Gaina.

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Gaina, C., Gaina, V. Polyimides with 3,3’-Bipyrrolidine-2,2’,5,5’-Tetrone Units. Polym. Bull. 59, 619–628 (2007). https://doi.org/10.1007/s00289-007-0805-6

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  • DOI: https://doi.org/10.1007/s00289-007-0805-6

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