Skip to main content
Log in

Monitoring of weathering and conservation of building materials through non-destructive X-ray computed microtomography

  • Original Article
  • Published:
Environmental Geology

Abstract

X-ray computed microtomography (µCT) is a promising non-destructive imaging technique based on measurements of the attenuation of X-rays. It provides information on the internal structure of small samples with a maximum resolution of 10 µm. For this study, two porous local natural building stones, the sandstone of Bray and the limestone of Maastricht, were selected. Possible applications of the µCT-technique for qualitative monitoring of changes comprise (1) to non-destructively determine porosity based on 3-D images, (2) to visualise weathering phenomena at the micron-scale, (3) to understand the rationale of weathering processes, (4) to visualise the presence of water repellents and consolidation products, (5) to monitor their protective effects during decay in order to understand the operating mechanisms and (6) to provide advise on the suitability of products for the treatment of a particular rock type. The µCT-technique proves to be a powerful monitoring tool for the future as the combination of 3-D visualisation and 3-D data provide new insights that could optimise conservation and restoration techniques of building materials.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

References

  • Breuls T (1994) Mergelgrotten, het onbekende landschap van Limburg. CIP-gegevens Koninklijke Bibliotheek, Den Haag

  • Carchon P (1986) Petrografie van de kalkstenen van het Krijt van Maastricht. Licentiate Thesis, Univ Gent, Faculty of Sciences

  • Clifton JR (1980) Stone consolidating materials — a status report

  • Cnudde V, Jacobs P, Vandenabeele P, De Witte I (2003) The potential of X-ray computed micro-tomography applied in conservation and restoration of natural building stones. In: Broekmans MATM, Jensen V, Brattli B, Proceedings 9th Euroseminar on Microscopy Applied to Building Materials, 9–12 September 2003, Trondheim, Norway

  • Cnudde V, Jacobs P (2004) Preliminary results of X-ray micro-tomography applied in conservation and restoration of natural building stones. X-ray CT for geomaterials: soils, concrete, rock. In: Otani J, Obare Y, Proceedings of the International Workshop on X-ray CT for Geomaterials, GeoX2003, 6–7 November 2003, Kumamoto, Japan: 363–371. A.A. Balkema Publishers

  • De Geyter G, Nijs R (1982) Petrografisch onderzoek van natuurlijke bouwstenen uit Belgische Tertiaire formaties. Het kwartsiet van Tienen (Formatie van Landen). Natuurwetenschappelijk Tijdschrift 64:41–59

    Google Scholar 

  • Diamond S (2000) Mercury porosimetry — an inappropriate method for the measurement of pore size distributions in cement-based materials. Cement Concrete Res 30:1517–1525

    Article  CAS  Google Scholar 

  • Felder WM, Bosch PW (2000) Krijt van Zuid-Limburg. Geologie van Nederland, deel 5. Nederlands Instituut voor Toegepaste Geowetenschappen TNO, Delft/Utrecht, Nederland

  • Jacobs P, Sevens E, Kunnen M (1995) Principles of computerised X-ray tomography and applications to building materials. Sci Total Environ 167:161–170

    Article  CAS  Google Scholar 

  • Ketcham RA, Carlson WD (2001) Acquisition, optimization and interpretation of X-ray computed tomographic imagery: applications to the geoscience. Computers Geosci 27(4):381–400

    Google Scholar 

  • Ministerie van het Waalse Gewest (1996) Pierres à bâtir traditionnelles de la Wallonie. Manuel de terrain

  • Nijs R (1985) Petrographical characterization of calcareous building stones in Northern Belgium. Vth International Congress on Deterioration and Conservation of Stone, Lausanne, 25–27 September 1985, pp 13–21

  • Perret J, Prasher SO, Kantzas A, Langford C (1999) Three-dimensional quantification of macropore networks in undisturbed soil cores. Soil Sci Soc Am J 63:1530–1543

    Google Scholar 

  • Price C (1996) Stone conservation. An overview of current research. Getty Conservation Institute, Los Angeles

  • RILEM (1980) Test No. 11.4, Water absorption under low pressure (pipe method), RILEM Commission 25-PEM, Tentative Recommendations

  • Soille P (1999) Morphological image analysis. Principles and applications. Springer, Berlin Heidelberg New York

  • Van Geet M (2001) Optimisation of microfocus X-ray computer tomography for geological research with special emphasis on coal components (macerals) and fractures (cleats) characterisation. PhD Thesis, KULeuven

  • Warscheid T, Braams J (2000) Biodeterioration of stone: a review. Int Biodeterior Biodegrad 46:343–368

    Article  CAS  Google Scholar 

  • WTCB Technische Voorlichting 205 (1997) Natuursteen,. September

  • WTCB Technische Voorlichting 224 (2002) Waterwerende oppervlaktebehandeling, June

  • Young ME, Cordiner P, Murray M (2003) Chemical consolidants and water repellents for sandstones in Scotland. Historic Scotland Research Report, ISBN 1-903570-20-4, pp 226

Download references

Acknowledgements

This study is supported by the Institute for the Promotion of Innovation by Science and Technology in Flanders, Belgium, through a PhD grant to V.C. The authors also thank Eric Pirard, Jean-Pierre Cnudde and Catherine Girard for their help in the development of the new software. The collaborators from FTB Restoration, Eddy De Witte (the Royal Institute for the Study and Conservation of Belgium’s Artistic Heritage) and Rolf De Bruyn, Yves Vanhellemont and Dominique Nicaise (Belgian Building Research Institute, BBRI) are acknowledged for their contribution in the research on water repellents, consolidants, weathering and restoration.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to P. J. S. Jacobs.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Cnudde, V., Jacobs, P.J.S. Monitoring of weathering and conservation of building materials through non-destructive X-ray computed microtomography. Env Geol 46, 477–485 (2004). https://doi.org/10.1007/s00254-004-1049-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00254-004-1049-5

Keywords

Navigation