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Chromatographic determination of phenylarsenic compounds

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Abstract

Gas chromatographic (GC) and liquid chromatographic methods for the investigation of phenylarsenic compounds are presented. With gas chromatography using an electron capture detector (ECD), the chemical warfare agents PFIFFIKUS, CLARK I and CLARK II can be detected. After derivatization with mercaptans and dimercaptans the sum of diphenylarsenic compounds resp. phenylarsenic and phenylarsonic compounds can be detected as the mercapto resp. dimercapto derivatives. High performance liquid chromatography (HPLC) analysis may be used for the detection of triphenylarsenic compounds and ADAMSITE.

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Authors and Affiliations

  1. Büro für Altlastenerkundung und Umweltforschung, Stadtwaldstrasse 45a, D-35037 Marburg, Germany, , , , , , DE

    R. Haas

  2. Environmental Hygiene and Immunology, Medical Centre of Hygiene, Philipps-University, Pilgrimstein 2, D-35037 Marburg, Germany, , , , , , DE

    Torsten C. Schmidt & Eberhard von Löw

  3. Department of Chemistry, Philipps-University, Hans-Meerwein-Strasse, D-35032 Marburg, Germany, , , , , , DE

    Klaus Steinbach

Authors
  1. R. Haas
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  2. Torsten C. Schmidt
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  3. Klaus Steinbach
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  4. Eberhard von Löw
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Received: 17 July 1997 / Accepted: 9 October 1997

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Haas, R., Schmidt, T., Steinbach, K. et al. Chromatographic determination of phenylarsenic compounds. Fresenius J Anal Chem 361, 313–318 (1998). https://doi.org/10.1007/s002160050892

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  • DOI: https://doi.org/10.1007/s002160050892

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