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Analytical and Bioanalytical Chemistry

, Volume 405, Issue 13, pp 4345–4352 | Cite as

Development challenges in the preparation of solution-based phytochemical and vitamin certified reference materials

  • Derrell JohnsonEmail author
  • Mitzi Rettinger
  • Tamara Tarbox
  • Beth Marek
  • Sherri Pogue
  • Isil Dilek
  • Uma Sreenivasan
Feature Article

Introduction

Reference materials serve a critical function in analytical testing by establishing a standardized basis for measurement or value assignment. ISO Guide 30 defines a reference material as a “[m]aterial or substance one or more of whose property values are sufficiently homogeneous and well established to be used for the calibration of an apparatus, the assessment of a measurement method, or for assigning values to materials” [1]. A Certified Reference Material (CRM), according to ISO Guide 34, is a “reference material characterized by a metrologically valid procedure for one or more specified properties, accompanied by a certificate that provides the value of the specified property, its associated uncertainty, and a statement of metrological traceability” [2]. For manufacture of active pharmaceutical ingredients, the US Food and Drug Administration (FDA) defines a primary reference standard as a “substance that has been shown by an extensive set of analytical tests to be...

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Copyright information

© Springer-Verlag Berlin Heidelberg 2013

Authors and Affiliations

  • Derrell Johnson
    • 1
    Email author
  • Mitzi Rettinger
    • 1
  • Tamara Tarbox
    • 1
  • Beth Marek
    • 1
  • Sherri Pogue
    • 1
  • Isil Dilek
    • 1
  • Uma Sreenivasan
    • 1
  1. 1.Cerilliant CorporationRound RockUSA

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