Abstract
A campaign to measure the amount of trace explosive residues in an operational military environment was conducted on May 27–31, 2007, at the National Training Center at Fort Irwin, CA, USA. The objectives of this campaign were to develop the methods needed to collect and analyze samples from tactical military settings, to use the data obtained to determine what the trace explosive signatures suggest about the potential capabilities of chemical-based means to detect IEDs, and, finally, to present a framework whereby a sound understanding of the signature science can be used to guide development of new sensing technologies and sensor concepts of operation. Through our use of combined background and threat signature data, we have performed statistical analyses to estimate upper limits of notional sensor performance that is limited only by the spatial correlation of the signature chemicals to the threats of interest.

















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References
Crowson CA, Cullum HE, Hiley RW, Lowe AM (1996) A survey of high explosives in public places. J Forensic Sci 41(6):980–989
Cullum HE, McGavigan C, Uttley CZ, Stroud MAM, Warren DC (2004) A second survey of explosive traces in public places. J Forensic Sci 40(4):1–7
Ostazeski SA, Oyler JM, Fountain AW III (2007) Edgewood Biological and Chemical Center, Analytical Test Report 0238-101507
EPA Method 8330B (SW-846): Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC), Revision 2, October 2006. Available from http://www.epa.gov/sam/pdfs/EPA-8330b.pdf. Accessed February 2007
EPA Method 8095 (SW-836): Explosives by gas chromatography, Revision 0. Available from http://www.epa.gov/sam/pdfs/EPA-8095.pdf. Accessed February 2007
Kunz RR, Clow KE, Hardy D, Switkes M, Krohn KE, Ostazeski SA, Oyler JM, Fountain AW III (2009) ECBC-TR-679, Quantitative analysis of trace explosive residues found at the National Training Center in Fort Irwin, CA, U.S. Army Edgewood Chemical and Biological Center, February
Oxley JC, Smith JL, Resende E, Pearce E (2003) Quantification and aging of the post-blast residue of TNT landmines. J Forensic Sci 48(4):1–12
Thompson RQ (1999) Aqueous recovery from cotton swabs of organic explosives followed by solid phase extraction. J Forensic Sci 44(4):795–804
Acknowledgments
The Lincoln Laboratory portion of this work was sponsored by JIEDDO/ECBC under Air Force Contract FA8721-050C-0002. Portions of this work, both in the laboratory and field, could not have been completed without the assistance of Dr. Michael Switkes and Mr. Keith Krohn of MIT-LL and Mr. Robert Calloway, Mr. John Sparks, Ms. Jennifer P. Exelby, Ms. Melissa Mullan, Mr. Tom Rusek (Battelle), Mr. J. Greene (Battelle), and Mr. Douglas Nichols (Battelle) of the ECBC, Forensics Analysis Center.
Opinions, interpretations, conclusions and recommendations are those of the authors and are not necessarily endorsed by the United States Government.
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Kunz, R.R., Gregory, K.C., Hardy, D. et al. Measurement of trace explosive residues in a surrogate operational environment: implications for tactical use of chemical sensing in C-IED operations. Anal Bioanal Chem 395, 357–369 (2009). https://doi.org/10.1007/s00216-009-2748-2
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DOI: https://doi.org/10.1007/s00216-009-2748-2
