Abstract
Recent studies have revealed the importance of powder transport by gas-phase flows in the laser-interaction zone in laser powder bed additive manufacturing. The understanding of such a mass transfer mechanism is necessary for developing and optimizing laser-assisted processes of additive manufacturing. Powder bed surface relief around the remelted track is experimentally characterized by metallography and laser scanning profilometry in single-track experiments with powders of various materials and various particle sizes. Denudation zones with sharp irregular boundaries containing particle agglomerates are observed for finer powders with smaller particles. Denudation zones without well-defined boundaries containing single particles are observed for coarser powders. The balance of forces applied to a particle is theoretically analyzed to understand powder rearrangement in the laser-interaction zone. The drag force is estimated by a similarity point-source model of the entrainment flow with a correction for the finite size of the evaporation spot. The adhesion force appears to be greater than the gravity one for the fine powders and lower than the gravity for the coarse powders, thus explaining the observed difference in the denudation zone morphology. The measured variation of the denudation width with the material properties and the particle size is consistent with the theoretical predictions.
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References
Gusarov AV, Grigoriev SN, Volosova MA, Melnik YA, Laskin A, Kotoban DV, Okunkova AA (2018) On productivity of laser additive manufacturing. J Mater Process Technol 261:213–232. https://doi.org/10.1016/j.jmatprotec.2018.05.033
Bouabbou A, Vaudreuil S (2022) Understanding laser-metal interaction in selective laser melting additive manufacturing through numerical modelling and simulation: a review. Virtual Phys Prototyp 17:1–20. https://doi.org/10.1080/17452759.2022.2052488
Yadroitsev I, Bertrand P, Smurov I (2006) Parametric analysis of selective laser melting technology, ICALEO 2006 Congress Proc 1825. https://doi.org/10.2351/1.5060792
Yadroitsev I, Bertrand Ph, Smurov I (2007) Parametric analysis of the selective laser melting process. Appl Surf Sci 253:8064–8069. https://doi.org/10.1016/j.apsusc.2007.02.088
Mumtaz KA, Hopkinson N (2010) Selective Laser Melting of thin wall parts using pulse shaping. J Mater Process Technol 210:279–287. https://doi.org/10.1016/j.jmatprotec.2009.09.011
Liu Y, Yang Y, Mai S, Wang D, Song C (2015) Investigation into spatter behavior during selective laser melting of AISI 316L stainless steel powder. Mater Des 87:797–806. https://doi.org/10.1016/j.matdes.2015.08.086
Gunenthiram V, Peyre P, Schneider M, Dal M, Coste F, Koutiri I, Fabbro R (2018) Experimental analysis of spatter generation and melt-pool behavior during the powder bed laser beam melting process. J Mater Process Technol 251:376–386. https://doi.org/10.1016/j.jmatprotec.2017.08.012
Matthews MJ, Guss G, Khairallah SA, Rubenchik A, Anderson AT, Depond PJ, King WE (2016) Denudation of metal powder layers in laser powder bed fusion processes. Acta Mater 114:33–42. https://doi.org/10.1016/j.actamat.2016.05.017
Ly S, Rubenchik AM, Khairallah SA, Guss G, Matthews MJ (2017) Metal vapor micro-jet controls material redistribution in laser powder bed fusion additive manufacturing. Sci Rep 7:4085. https://doi.org/10.1038/s41598-017-04237-z
Bidare P, Bitharas I, Ward RM, Attallah MM, Moore AJ (2018) Fluid and particle dynamics in laser powder bed fusion. Acta Mater 142:107–120. https://doi.org/10.1016/j.actamat.2017.09.051
Zhirnov I, Kotoban DV, Gusarov AV (2018) Evaporation-induced gas-phase flows at selective laser melting. Appl Phys A 124:157. https://doi.org/10.1007/s00339-017-1532-y
Volpp J (2019) Powder particle movement during powder bed fusion. Procedia Manuf 36:26–32. https://doi.org/10.1016/j.promfg.2019.08.005
Zhao C, Fezzaa K, Cunningham RW, Wen H, De Carlo F, Chen L, Rollett AD, Sun T (2017) Real-time monitoring of laser powder bed fusion process using high-speed X-ray imaging and diffraction. Sci Rep 7:3602. https://doi.org/10.1038/s41598-017-03761-2
Guo Q, Zhao C, Escano LI, Young Z, Xiong L, Fezzaa K, Everhart W, Brown B, Sun T, Chen L (2018) Transient dynamics of powder spattering in laser powder bed fusion additive manufacturing process revealed by in-situ high-speed high energy x-ray imaging. Acta Mater 151:169–180. https://doi.org/10.1016/j.actamat.2018.03.036
Gusarov AV (2020) Entrainment flow of a jet emerging into a half-space with the no-slip boundary condition. Phys Fluids 32:083107. https://doi.org/10.1063/5.0015040
Bidare P, Bitharas I, Ward RM, Attallah MM, Moore AJ (2018) Laser powder bed fusion at sub-atmospheric pressures. Int J Mach Tools Manuf 130–131:65–72. https://doi.org/10.1016/j.ijmachtools.2018.03.007
Bidare P, Bitharas I, Ward RM, Attallah MM, Moore AJ (2018) Laser powder bed fusion in high-pressure atmospheres. Int J Adv Manuf Technol 99:543–555. https://doi.org/10.1007/s00170-018-2495-7
Zauner E (1985) Visualization of the viscous flow induced by a round jet. J Fluid Mech 154:111–119. https://doi.org/10.1017/S0022112085001446
Schneider W (1981) Flow induced by jets and plumes. J Fluid Mech 108:55–65. https://doi.org/10.1017/S0022112081001985
Schneider W (1985) Decay of momentum flux in submerged jets. J Fluid Mech 154:91–110. https://doi.org/10.1017/S0022112085001434
Anisimov SI (1968) Vaporization of metal absorbing laser radiation. Sov Phys JETP 27:182–183
Gusarov AV, Smurov I (2002) Gas-dynamic boundary conditions of evaporation and condensation: numerical analysis of the Knudsen layer. Phys Fluids 14:4242. https://doi.org/10.1063/1.1516211
Lemanov VV, Terekhov VI, Sharov KA, Shumeiko AA (2013) An experimental study of submerged jets at low Reynolds numbers. Tech Phys Lett 39:421–423. https://doi.org/10.1134/S1063785013050064
Masmoudi A, Bolot R, Coddet C (2015) Investigation of the laser-powder-atmosphere interaction zone during the selective laser melting process. J Mater Process Technol 225:122–132. https://doi.org/10.1016/j.jmatprotec.2015.05.008
Mayi YA, Dal M, Peyre P, Bellet M, Metton C, Moriconi C, Fabbro R (2020) Laser-induced plume investigated by finite element modelling and scaling of particle entrainment in laser powder bed fusion. J Phys D 53:075306. https://doi.org/10.1088/1361-6463/ab5900
Chen H, Yan W (2020) Spattering and denudation in laser powder bed fusion process: multiphase flow modelling. Acta Mater 196:154–167. https://doi.org/10.1016/j.actamat.2020.06.033
Li X, Zhao C, Sun T, Tan W (2020) Revealing transient powder-gas interaction in laser powder bed fusion process through multi-physics modeling and high-speed synchrotron x-ray imaging. Addit Manuf 35:101362. https://doi.org/10.1016/j.addma.2020.101362
Amiri M, Payton EJ (2021) An analytical model for prediction of denudation zone width in laser powder bed fusion additive manufacturing. Addit Manuf 48:102461. https://doi.org/10.1016/j.addma.2021.102461
EL-Amin MF, Sun S, Heidemann W, Muller-Steinhagen H (2010) Analysis of turbulent buoyant confined jet modeled using realizable k–ε model. Heat Mass Transf 46:943–960. https://doi.org/10.1007/s00231-010-0625-3
Gusarov AV (2020) Analytic similarity solutions of the Navier-Stokes equations for a jet in a half space with the no-slip boundary condition. Phys Fluids 32:053104. https://doi.org/10.1063/5.0008111
Kaserer L, Bergmueller S, Braun J, Leichtfried G (2020) Vacuum laser powder bed fusion - track consolidation, powder denudation, and future potential. Int J Adv Manuf Technol 110:3339–3346. https://doi.org/10.1007/s00170-020-06071-6
Traore S, Schneider M, Koutiri I, Coste F, Fabbro R, Charpentier C, Lefebvre P, Peyre P (2021) Influence of gas atmosphere (Ar or He) on the laser powder bed fusion of a Ni-based alloy. J Mater Process Technol 288:116851. https://doi.org/10.1016/j.jmatprotec.2020.116851
Ferziger JH, Kaper HG (1972) Mathematical theory of transport processes in gases, North-Holland
Achee T, Guss G, Elwany A, Matthews M (2021) Laser pre-sintering for denudation reduction in the laser powder bed fusion additive manufacturing of Ti-6Al-4V alloy. Addit Manuf 42:101985. https://doi.org/10.1016/j.addma.2021.101985
Zhao Y, Aoyagi K, Yamanaka K, Chiba A (2020) Role of operating and environmental conditions in determining molten pool dynamics during electron beam melting and selective laser melting. Addit Manuf 36:101559. https://doi.org/10.1016/j.addma.2020.101559
Khmyrov RS, Protasov CE, Grigoriev SN, Gusarov AV (2016) Crack-free selective laser melting of silica glass: single beads and monolayers on the substrate of the same material. Int J Adv Manuf Technol 85:1461–1469. https://doi.org/10.1007/s00170-015-8051-9
Khmyrov RS, Ableeva RR, Gusarov AV (2020) Metallographic study of denudation in laser powder-bed fusion. Procedia CIRP 94:194–199. https://doi.org/10.1016/j.procir.2020.09.037
Oerlikon Metco (2022) https://www.oerlikon.com
Grigoriev IS, Meilikhov EZ (1997) Handbook of physical quantities. CRC Press, New York
LMI Technologies (2022) https://lmi3d.com/series/mikrocad-series/
Leite FL, Bueno CC, Da Róz AL, Ervino Ziemath EC, Oliveira ON Jr (2012) Theoretical models for surface forces and adhesion and their measurement using atomic force microscopy. Int J Mol Sci 13:12773–856. https://doi.org/10.3390/ijms131012773
Hibbeler RC (2016) Engineering mechanics: statics and dynamics. Pearson, New York
Yadroitsev I, Gusarov A, Yadroitsava I, Smurov I (2010) Single track formation in selective laser melting of metal powders. J Mater Process Technol 210:1624–1631. https://doi.org/10.1016/j.jmatprotec.2010.05.010
Ciurana J, Hernandez L, Delgado J (2013) Energy density analysis on single tracks formed by selective laser melting with CoCrMo powder material. Int J Adv Manuf Technol 68:1103–1110. https://doi.org/10.1007/s00170-013-4902-4
Bergström L (1997) Hamaker constants of inorganic materials. Adv Colloid Interface Sci 70:125–169. https://doi.org/10.1016/S0001-8686(97)00003-1
Eichenlaub S, Chan C, Beaudoin SP (2002) Hamaker constants in integrated circuit metalization. J Colloid Interface Sci 248:389–397. https://doi.org/10.1006/jcis.2002.8241
Tolias P (2018) Lifshitz calculations of Hamaker constants for fusion relevant materials. Fusion Eng Des 133:110–116. https://doi.org/10.1016/j.fusengdes.2018.06.002
Meier C, Weissbach R, Weinberg J, Wall WA, Hart AJ (2019) Critical influences of particle size and adhesion on the powder layer uniformity in metal additive manufacturing. J Mater Process Technol 266:484–501. https://doi.org/10.1016/j.jmatprotec.2018.10.037
Andersson KM, Bergström L (2002) DLVO interactions of tungsten oxide and cobalt oxide surfaces measured with the colloidal probe technique. J Colloid Interface Sci 246:309–315. https://doi.org/10.1006/jcis.2001.8021
Funding
This work was supported by the Russian Science Foundation (grant agreement no. 21–79-30058). The experiments were carried out using the equipment of the Centre of collective use of MSUT “STANKIN” supported by the Ministry of Science and Higher Education of the Russian Federation (contract no. 075–15-2021–695).
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Conceptualization SG, AG. Investigation AK, RK, TT. Supervision AG. Data curation RA, AK. Funding acquisition SG. Writing–original draft RK, AG. Writing–review and editing SG, AK, TT.
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Grigoriev, S., Ableyeva, R., Korotkov, A. et al. Powder bed surface relief formation and denudation in selective laser melting. Int J Adv Manuf Technol 123, 543–558 (2022). https://doi.org/10.1007/s00170-022-10197-0
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DOI: https://doi.org/10.1007/s00170-022-10197-0