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A study of densification and phase transformations of nanocomposite Cu-Fe prepared by mechanical alloying and consolidation process

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Abstract

The purpose of this study is an attempt to obtain nanocrystalline bulk Cu-40 at.% Fe alloy by mechanical alloying followed by consolidation process under 7 GPa and annealing. The transformations occurring in the material were studied by the use of X-ray diffraction. The structural investigations revealed that consolidation enabled supersaturated Cu(Fe) to precipitate out Cu4Fe and CuFe4 intermetallics. A limited grain growth was noticed after annealing. The results of microhardness have shown that the hardening increases similarly up to 40 h milling. The variation of microhardness as a function of the reciprocal square root of the grain size demonstrates that the rate of hardening is similar to that predicted by the Hall-Petch behavior.

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References

  1. Suryanarayana C (2001) Mechanical alloying and milling. Prog Mater Sci 46:1–184

    Article  Google Scholar 

  2. Kim TS, Ryu JY, Lee JK, Bae JC (2007) Synthesis of Cu-base/Ni-base amorphous powder composites. Mater Sci Eng A 449(451):804–808

    Article  Google Scholar 

  3. Straumal BB, Mazilkin AA, Baretzky B, Schütz G, Rabkin E, Valiev RZ (2012) Accelerated diffusion and phase transformations in CoCu alloys driven by the severe plastic deformation. Mater Trans 53(1):63–71

    Article  Google Scholar 

  4. Chao J, Morris DG, Munoz-Morris MA, Gonzalez-Carrasco JL (2001) The influence of some microstructural and test parameters on the tensile behaviour and the ductility of a mechanically-alloyed Fe-40Al alloy. Intermetallics 9(4):299–308

    Article  Google Scholar 

  5. Kransnowski M, Kulik T (2010) Bulk amorphous and nanocrystalline Al83Fe17 alloys prepared by consolidation of mechanically alloyed amorphous powder. J Alloys Compd 495:382–385

    Article  Google Scholar 

  6. Yavari AR, Botta Filho WJ, Rodrigues CAD, Cardoso C, Valiev RZ (2002) Nanostructured bulk Al90Fe5Nd5 prepared by cold consolidation of gas atomised powder using severe plastic deformation. Scr Mater 46:711–716

    Article  Google Scholar 

  7. Mhadhbi M, Khitouni M, Escoda L, Sunol JJ, Dammak M (2011) Microstructure evolution and mechanical properties of nanocrystalline FeAl obtained by mechanical alloying and cold consolidation. J Alloys Compd 509:3293–3298

    Article  Google Scholar 

  8. Rawers J (1999) Comparison of attrition milled nanostructured, powder-compaction techniques. Nano Structured Materials 11(4):513–522

    Article  Google Scholar 

  9. Mohamed FA (2003) A dislocation model for the minimum grain size obtainable by milling. Acta Mater 51:4107–19

    Article  Google Scholar 

  10. Mhadhbi M, Khitouni M, Azabou M, Kolsi A (2008) Characterization of Al and Fe nanosized powders synthesized by high energy mechanical milling. J Mater Charac 59:944

    Article  Google Scholar 

  11. Salimon AI, Korsunsky AM, Ivanov AN (1999) The character of dislocation structure evolution in nanocrystalline FCC Ni-Co alloys prepared by high-energy mechanical milling. J Mater Sci Eng A 271:196–205

    Article  Google Scholar 

  12. Fecht HJ (1995) Nanostructure formation by mechanical attrition. Nanostruct Mater 6(1–4):33–42

    Article  Google Scholar 

  13. Gaffet E, Le Caër G, in: Nalwa HS (Ed.) (2004) Mechanical processing for nanomaterials, Encyclopedia of Nanoscience and Nanotechnology, 5, American Scientific Publishers, 91

  14. Zhao YH, Sheng HW, Lu K (2001) Microstructure evolution and thermal properties in nanocrystalline Fe during mechanical attrition. Acta Mater 49:365

    Article  Google Scholar 

  15. Mhadhbi M, Khitouni M, Escoda L, Suñol JJ (2010) Studies of structure defects in nanostructured FeAl alloy. J Mater Letters 64:1802

    Article  Google Scholar 

  16. Kransnowski M, Kulik T (2003) FeAl-TiN nanocomposite produced by reactive ball milling and hot-pressing consolidation. Scipta Materialia 48:1489–1494

    Article  Google Scholar 

  17. Morris MA, Lebouf M (1997) Grain-size refinement of γ-Ti-Al alloys: effect on mechanical properties. Mater Sci Eng A224:1

    Article  Google Scholar 

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Correspondence to M. Khitouni.

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Azabou, M., Makhlouf, T., Saurina, J. et al. A study of densification and phase transformations of nanocomposite Cu-Fe prepared by mechanical alloying and consolidation process. Int J Adv Manuf Technol 87, 981–987 (2016). https://doi.org/10.1007/s00170-016-8551-2

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  • DOI: https://doi.org/10.1007/s00170-016-8551-2

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