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A study of densification and on factors affecting the density of Ni x –Fe100 − x nanopowders prepared by mechanical alloying and sintered by spark plasma

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Abstract

Mechanical alloying through high-energy ball milling was used in the production of Ni–Fe alloy powders from elemental Ni and Fe powders of average particle size 80 and 25 μm, respectively. High-energy planetary ball milling at room temperature was performed for various time durations ranging between 2 and 100 h. SPS apparatus was used for sintering of powder particles. Density of all specimens was reported and a maximum densification of 99 % was achieved in 50 wt.% Ni–Fe milled for 16 h prior to spark plasma sintering at 1,223 K.

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References

  1. Chryssolouris G, Stavropoulos P, Tsoukantas G, Salonitis K, Stournaras A (2004) Nanomanufacturing processes: a critical review. Int J Mater Prod Technol 21(4):331–348

    Article  Google Scholar 

  2. Barrett WF, Brown W, Hadfield RA (1902) Researches on the electrical conductivity and magnetic properties of upwards of one hundred different alloys of iron. Inst Elec Eng J 31:674–729

    Google Scholar 

  3. Miura H, Isa S, Omuro K (1990) Preparation of iron–nickel based metal–metalloid amorphous powders by mechanical alloying. J Non-Cryst Solids 117–118(Part 2):741–744

    Article  Google Scholar 

  4. Ivanov E (1992) Preparation of Cu x Hg1 − x solid solutions by mechanical alloying. Mater Sci Forum 88–90:475–480

    Article  Google Scholar 

  5. Yavari AR, Desré PJ, Benameur T (1992) Mechanically driven alloying of immiscible elements. Phys Rev Lett 68(14):2235–2238

    Article  Google Scholar 

  6. Niihara K (1991) New design concept of structural ceramics―ceramic nanocomposites. J Ceram Soc Jpn 99(10):974–982

    Article  Google Scholar 

  7. Perera DS, Tokita M, Moricca S (1998) Comparative study of fabrication of Si3N4/SiC composites by spark plasma sintering and hot isostatic pressing. J Eur Ceram Soc 18(4):401–404

    Article  Google Scholar 

  8. Gao L, Wang HZ, Hong JS, Miyamoto H, Miyamoto K, Nishikawa Y, Torre SDDL (1999) Mechanical properties and microstructure of nano-SiC–Al2O3 composites densified by spark plasma sintering. J Eur Ceram Soc 19(5):609–613

    Article  Google Scholar 

  9. Zhang HW, Gopalan R, Mukai T, Hono K (2005) Fabrication of bulk nanocrystalline Fe–C alloy by spark plasma sintering of mechanically milled powder. Scr Mater 53(7):863–868

    Article  Google Scholar 

  10. Gopalan R, Kündig AA, Ohnuma M, Kishimoto S, Hono K (2005) Mechanically milled and spark plasma sintered FePt-based bulk magnets with high coercivity. Scr Mater 52(8):761–765

    Article  Google Scholar 

  11. Biswas K, Mukhopadhyay A, Basu B, Chattopadhyay K (2007) Densification and microstructure development in spark plasma sintered WC–6 wt % ZrO2 nanocomposites. J Mater Res 22(6):1491–1501

    Article  Google Scholar 

  12. Kar S, Sarma ES, Somu VB, Kishore NK, Srinivas V (2008) Evaluation of different consolidation methods for nano-materials. Indian J Eng Mater Sci 15(4):343–346

    Google Scholar 

  13. Scherrer P (1918) Göttinger Nachrichten Gesell 2:98

    Google Scholar 

  14. Williamson GK, Hall WH (1953) X-ray line broadening from filed aluminium and wolfram. Acta Metall 1(1):22–31

    Article  Google Scholar 

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Correspondence to Thanganadar Ashokkumar.

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Ashokkumar, T., Rajadurai, A., Gouthama et al. A study of densification and on factors affecting the density of Ni x –Fe100 − x nanopowders prepared by mechanical alloying and sintered by spark plasma. Int J Adv Manuf Technol 65, 1201–1213 (2013). https://doi.org/10.1007/s00170-012-4247-4

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  • DOI: https://doi.org/10.1007/s00170-012-4247-4

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