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Determination of Diacylhydrazines-Type Insect Growth Regulator JS-118 Residues in Cabbage and Soil by High Performance Liquid Chromatography with DAD Detection

Abstract

JS-118 is a diacylhydrazines-type insect growth regulator used extensively in China now. An analytical method for residues determination of JS-118 in cabbage and soil samples by high performance liquid chromatography with DAD detection was established and optimized. Primary secondary amine solid phase extraction cartridge was used for sample preparation. Mean recoveries for the analyte ranged from 96.6% to 107.0% with CV value less than 4.7%. The limit of quantification is 0.01 mg/kg. Direct confirmation of JS-118 residues in samples was realized by high performance liquid chromatography-mass spectrometry. The proposed method is simple, rapid and reliable to perform and could be utilized for monitoring of pesticides residues.

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References

  1. Hu JY, Yan H (2008) Determination of flumorph residues in vegetables, soil and natural water by solid phase extraction cleanup and high performance liquid chromatography with UV detection. J AOAC Int 91:1459–1466

    CAS  Google Scholar 

  2. Hu JY, Liu C, Zhang YC, Zheng ZX (2009) Hydrolysis and photolysis of diacylhydrazines-type insect growth regulator JS-118 in aqueous solutions under abiotic conditions. Bull Environ Contam Toxicol 82:610–615

    Article  CAS  Google Scholar 

  3. Li JZ, Hu JY (2006) Analysis of Forchlorfenuron residues in watermelon by solid phase extraction and high-performance liquid chromatography. J AOAC Int 89:1635–1640

    Google Scholar 

  4. Zhang XN (2005) Novel insect growth regulator Funanchongxianjing (JS-118). World Pestic 27:48–49

    Google Scholar 

Download references

Acknowledgments

This work was supported by the financial support of National Natural Science Foundation of China (No. 20777078).

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Correspondence to J.-Y. Hu.

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Hu, JY., Deng, ZB. & Qin, DM. Determination of Diacylhydrazines-Type Insect Growth Regulator JS-118 Residues in Cabbage and Soil by High Performance Liquid Chromatography with DAD Detection. Bull Environ Contam Toxicol 83, 803 (2009). https://doi.org/10.1007/s00128-009-9831-4

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Keywords

  • JS-118
  • Residues determination
  • Solid phase extraction
  • HPLC-DAD