An immunoaffinity chromatography column was developed to remove diazinon from water and soil samples. In this paper, two types of absorbent columns, the immunoaffinity chromatography column and the ENVI-Carb column, were compared. To accomplish this, each of these columns was used to treat water and soil samples that had been spiked with diazinon at concentrations of 2.5 or 5 ng/mL (or ng/g). High performance liquid chromatography was then used to analyze the treated samples. The ENVI-Carb column recovered 87.99%–95.95% of the diazinon from water and soil with CVs of 5.08%–8.06%. The recoveries observed when the immunoaffinity chromatography column was used were slightly lower (52.61%–81.58%); however, it effectively clean up the soil samples.
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This work was supported by the Chinese National “863” High-Tech Research Program (2006AA10Z450).
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Tang, J., Zhang, M., Cheng, G. et al. Diazinon Determination Using High Performance Liquid Chromatography: A Comparison of the ENVI-Carb Column with the Immunoaffinity Column for the Pretreatment of Water and Soil Samples. Bull Environ Contam Toxicol 83, 626 (2009). https://doi.org/10.1007/s00128-009-9823-4
- Solid phase extraction