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Solid State Cleavage of Semicarbazones with Montmorillonite K-10 Supported Bis(trimethylsilyl)chromate under Microwave Irradiation

Mikrowellenunterstützte Spaltung von Semicarbazonen mit an Montmorillonit K-10 adsorbiertem Bis(trimethylsilyl)chromat im Festkörper

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Summary.

 Semicarbazones of aldehydes and ketones adsorbed on clay can be cleaved oxidatively to the corresponding carbonyl compounds under solvent-free conditions in high yields employing bis(trimethylsilyl)chromate and microwave irradiation.

Zusammenfassung.

 An Ton adsorbierte Semicarbazone von Aldehyden und Ketonen können mit Bis(trimethylsilyl)chromat unter Bestrahlung mit Mikrowellen in einer Festphasenreaktion in hohen Ausbeuten oxidativ zu den ensprechenden Carbonylverbindungen gespalten werden.

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Authors and Affiliations

  1.  Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran, IR

    Majid M. Heravi & Dariush Ajami

  2.  Department of Chemistry, University of Mazandaran, Babolsar, Iran, IR

    Mahmood Tajbakhsh & Hamid Bakooie

Authors
  1. Majid M. Heravi
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  2. Mahmood Tajbakhsh
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  3. Hamid Bakooie
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  4. Dariush Ajami
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Additional information

Received August 21, 1998. Accepted October 7, 1998

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Heravi, M., Tajbakhsh, M., Bakooie, H. et al. Solid State Cleavage of Semicarbazones with Montmorillonite K-10 Supported Bis(trimethylsilyl)chromate under Microwave Irradiation. Monatshefte fuer Chemie 130, 933–936 (1999). https://doi.org/10.1007/PL00010275

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  • DOI: https://doi.org/10.1007/PL00010275

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