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Metal-Template Synthesis and Characterization of a Nitrogen-Oxygen Donor Schiff Base Macrocyclic System

Metallunterstuützte Synthese und Charakterisierung eines makrocyclischen Stickstoff-Sauerstoff-Donor-Liganden

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Summary.

 Reaction of 2,6-diacetylpyridine with 1,12-diamine-4,9-dioxadodecane in the presence of magnesium(II), zinc(II), and cadmium(II) perchlorates as template agents gives the complexes of 19-membered macrocyclic ligand 1 with a set of two N and three O donor atoms. The complexes were characterized by spectroscopic methods (IR, 1H NMR, FAB-MS) and thermogravimetric and elemental analyses.

Zusammenfassung.

 Reaktion von 2,6-Diacetylpyridin mit 1,12-Diamin-4,9-dioxadodecan in Gegenwart von Magnesium(II)-, Zink(II)- und Cadmium(II)perchlorat ergibt die entsprechenden Komplexe des 19-gliedrigen Makrocyclus 1, der über 5 Donoratome verfügt (3×N, 2×O). Die Komplexe wurden mit spektroskopischen Methoden (IR, 1H-NMR, FAB-MS) sowie mittels thermogravimetrischer Analyse und Elementaranalyse charakterisiert.

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Authors and Affiliations

  1. Faculty of Chemistry, Adam Mickiewicz University, PL-60780 Poznań, Poland, PL

    Violetta Patroniak-Krzyminiewska, Hanna Litkowska & Wanda Radecka-Paryzek

Authors
  1. Violetta Patroniak-Krzyminiewska
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  2. Hanna Litkowska
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  3. Wanda Radecka-Paryzek
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Received April 20, 1998. Accepted (revised) May 26, 1998

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Patroniak-Krzyminiewska, V., Litkowska, H. & Radecka-Paryzek, W. Metal-Template Synthesis and Characterization of a Nitrogen-Oxygen Donor Schiff Base Macrocyclic System. Monatshefte fuer Chemie 130, 243–247 (1999). https://doi.org/10.1007/PL00010204

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  • DOI: https://doi.org/10.1007/PL00010204

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