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The crystal and molecular structure of a clip-shaped molecule with two different side-walls

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Abstract

The crystal and molecular structure of a clip-shaped molecule is described. The structure was solved by vector search methods and refined by least squares methods to R1 = 0.0769 [I > 2σ(I)]. Crystal data: C40H36N4O6.2CCl3H, monoclinic, space group P21/n, a = 12.567(1), b = 19.171(1), c = 17.431(1)Å β = 91.676(6)°, V = 4197.7(5)Å3, Z = 4.

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Authors and Affiliations

  1. Department of Organic Chemistry, Nijmegen SON Research Center, University of Nijmegen, Toemooiveld, 6525 ED, Nijmegen, The Netherlands

    J. N.H. Reek, J. A. A. W. Elemans & R. J. M. Nolte

  2. Department of Inorganic Chemistry, Nijmegen SON Research Center, University of Nijmegen, Toemooiveld, 6525 ED, Nijmegen, The Netherlands

    J. M. M. Smits & R. de Gelder

  3. RIM Laboratory of Solid State Chemistry, University of Nijmegen, Toemooiveld, 6525 ED, Nijmegen, The Netherlands

    W. P. Bosman

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  1. W. P. Bosman
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  2. J. M. M. Smits
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  3. R. de Gelder
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  4. J. N.H. Reek
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  5. J. A. A. W. Elemans
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  6. R. J. M. Nolte
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Bosman, W.P., Smits, J.M.M., de Gelder, R. et al. The crystal and molecular structure of a clip-shaped molecule with two different side-walls. J Chem Crystallogr 27, 75–79 (1997). https://doi.org/10.1007/BF03543091

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  • DOI: https://doi.org/10.1007/BF03543091

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