Skip to main content
Log in

Zone purification of reactive metals

  • Published:
JOM Aims and scope Submit manuscript

Abstract

A description is given for an apparatus and technique used to zone melt reactive, high-melting-point metals by the floating zone method. The use of radioactive tracers to determine the redistribution of solute during zone melting is discussed and results are shown for P32 in iron, Au198 in titanium and zirconium, and Zn65 in titanium. Some tensile results on iron at liquid nitrogen and liquid helium temperatures are given which indicate that the removal of trace impurities markedly increase the low temperature ductility of iron.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. W. G. Pfann: AIME Trans., 1952, vol. 194, p. 747; Journal of Metals, July 1952.

    Google Scholar 

  2. H. Theurer: Unpublished research.

  3. P. H. Keck and M. J. E. Golay: Physical Review, 1953, vol. 89, p. 1297.

    Article  Google Scholar 

  4. P. H. Keck, W. Van Horn, J. Solad, and A. MacDonald: Review of Scientific Instruments, 1954, vol. 23, p. 331.

    Article  Google Scholar 

  5. P. A. Albert, F. Montariol, R. Reich, and G. Chaudron: Radioisotope Conference, 1954, vol. 2, p. 75.

    Google Scholar 

  6. L. Burris, Jr., C. Stockman, and I. Villon: AIME Trans., 1955, vol. 203, p. 1017; Journal of Metals, September 1955.

    Google Scholar 

  7. R. L. Smith, G. Spangler, and R. M. Brick: ASM Trans., 1954, vol. 46, p. 973.

    Google Scholar 

  8. R. L. Smith and J. L. Rutherford: To be published.

  9. L. Seigle and R. M. Brick: ASM Trans., 1948, vol. 40, p. 813.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Additional information

TP 4424E. Manuscript, Apr. 13, 1956. Buffalo Regional Reactive Metals Conference, March 1956.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Smith, R.L., Rutherford, J.L. Zone purification of reactive metals. JOM 9, 478–484 (1957). https://doi.org/10.1007/BF03397903

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF03397903

Navigation