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Bestimmung der Fumonisine FB1 und FB2 sowie ihrer hydrolisierten Metaboliten mittels HPLC-ESI-MS

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Abstract

A rapid determination of fumonisins FB1, FB2 and hydrolyzed fumonisins HFB1, HFB2 in maize products is possible by application of high-performance liquid chromatography in combination with electrospray ionization mass spectrometry (HPLC-ESI-MS). Without any additional clean up or purification of the sample extract a quantitation limit of 20 μg/kg sample with a signal to noise ratio of 10∶1 was observed.

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Literaturverzeichnis

  1. Sydenham E W, Stockenström S, Thiel P G, Shephard G S, Koch K R, Marasas W F O (1995) Potential of Alkaline Hydrolysis for the Removal of Fumonisins from Contaminated Corn. J. Agric. Food Chem. 43: 1198–1201.

    Article  CAS  Google Scholar 

  2. Sydenham E W, Thiel P G, Marasas W F O, Shephard G S, Van Schalkwyk D J, Koch K R (1990) Natural occurrence of some Fusarium mycotoxins in corn from low and high esophageal cancar prevalence areas of the Transkei, Southern Africa. J. Agric. Food Chem. 38: 1900–1903.

    Article  CAS  Google Scholar 

  3. Hendrich S, Miller K A, Wilson T M, Murphy P M (1993) Toxicity of Fusarium proliferatum-fermented nixtamalized corn-based diets fed to rats. J. Agric. Food Chem. 41: 1649–1654.

    Article  CAS  Google Scholar 

  4. Shephard G S (1998) Chromatographic determination of the fumonisin mycotoxins. J. Chromatogr. A 815: 31–39.

    Article  CAS  PubMed  Google Scholar 

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Brockmeyer, A., Thielert, G. Bestimmung der Fumonisine FB1 und FB2 sowie ihrer hydrolisierten Metaboliten mittels HPLC-ESI-MS. Mycotox Res 17 (Suppl 1), 112–115 (2001). https://doi.org/10.1007/BF03036724

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