Abstract
The preparation of silver nanoparticles by the reduction of AgNO3 with hydrazine in lgepal CO-520/cyclohexane reverse micelle solutions has been studied. Transmission electron microscope, electron diffraction, and X-ray diffraction pattern analyses revealed the resultant particles to be silver. The average size of the synthesized nanoparticles first increased and thereafter approached a constant value with increased molar ratio of water to Igepal CO 520 and with increasing concentration of AgNO3.
Similar content being viewed by others
References
I. Sondi, D. V. Goia, and E. Matijevic,J. Colloid. Intef. Sci. 260, 75 (2003).
R. Pool,Science 248, 1186 (1990).
Y. Wang and N. Herron,J. Phys. Chem. 95, 525 (1991).
Z. Zhang, B. Zhao, and L. Hu,J. Solid State Chem. 121, 105 (1996).
K. S. Chou and C. Y. Ren,Mater. Chem. Phys. 64, 241 (2000).
Y. Zhu, Y. Qian, M. Zhang, and Z. Chen,Mater. Lett. 17, 314 (1993).
H. S. Zhou, T. Wada, H. Sasabe, and H. Komiyama,Appl. Phys. Lett. 68, 1288 (1996).
Y. A. Kotov and O. M. Samatov,Acta metall. 12, 119 (1999).
K. Okitsu, H. Bandow, and Y. Maeda,Chem. Mater. 8, 315 (1996).
P. Y. Silver, R. Herrera-Urbina, N. Duvauchelle, and V. Vijayakrishnan,J. Mater. Chem. 6, 573 (1996).
D. S. Bae, S. W. Park, K. S. Han, and J. H. Adair,Met. Mater.-Int. 7, 399 (2001).
M. P. Pileni,Structure and Reactivity in Reverse Micelles, Elsevier, Amsterdam (1989).
B. K. Paul and S. P. Moulik,J. Dispersion Sci. Technol. 18, 301 (1997).
K. Osseo-Asare and F. J. Arriagada,Ceram. Trans. 12, 3 (1990).
M. P. Pileni,J. Phys. Chem. 97, 6961 (1993).
V. Pillai, P. Kumar, M. J. Hou, P. Ayyub, and D. O. Shah,Adv. Colloid Interface Sci. 55, 241 (1995).
J. Rouviere, J. M. Couret, M. Lindheimer, J. L. Dejardin, and R. Marrony,J. Chem. Phys. 76, 289 (1979).
Ph. Monnoyer, A. Fonseca, and J. B. Nagy,Colloid. Surf. A: Physicochemical Eng. Aspects 100, 233 (1995).
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Bae, DS., Kim, EJ., Bang, JH. et al. Synthesis and characterization of silver nanoparticles by a reverse micelle process. Met. Mater. Int. 11, 291–294 (2005). https://doi.org/10.1007/BF03027331
Issue Date:
DOI: https://doi.org/10.1007/BF03027331