Abstract
The combination of Gas chromatography (GC) for separation and Flame Ionization Detection (FID) for detection and identification of the components of a mixture of compounds is a fast and strongly proved method of analytic chemistry. The objective of this research was to design a combined High-speed miniature screening Gas chromatograph along with a Flame Ionization Detector for quick, quantitative and qualitative analysis of gas components. This combined GC-FID system is suitable to detect the volatile and semi-volatile hydrocarbons present in a gas mixture. The construction made it less expensive, easy to use and movable. The complete gas path was developed. On/off valves, temperature and flow sensors and their interface electronics were used for controlling purpose. A Microcontroller was programmed to measure the temperature and gas flow using the sensors and to control and regulate them using the electronics and valves. A pocket PC with its touch screen served as a user interface for the system. Software was developed for the pocket PC, which makes the communication possible with the Microcontroller. The system parameters can be indicated in the Pocket PC as simple text and also the analysis result can be displayed.
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References
Ernst Kenndler, 1999, “Introduction to Chromatography,” University of Vienna.
Hicham Dakir, 2001, “Aufbau und Steuerung Eines Hochgeschwindigkeits-Gaschromatographen Mit Integriertem Anreicherungsmodul Fur Ein Mobiles Massenspektrometer,” Studienarbeit, Technical University of Hamburg-Harburg, Dept. of Measurement Engineering.
Kyunghyun Ryu and Youngtaig Oh, 2003, “A Study on the Usability of Biodiesel Fuel Derived from Rice Bran Oil as an Alternative Fuel for IDI Diesel Engine,”KSME International Journal, Vol 17, No. 2, pp. 310–317.
Lars Bilke, 2002, “Mikrocontrollergesteuerter Thermodesorber fur die Analyse schwerfluchtiger Abgaskomponenten,” Diplomarbeit, Technical University of Hamburg-Harburg, Dept. of Measurement Engineering.
Rahul Banik, 2003, “Construction and Control of a High Speed Miniature Screening Gaschromatography with a Flame Ionization Detector,” Diplomarbeit, Technical University of Hamburg-Harburg, Dept. of Measurement Engineering.
Rather, O., 1993. “Analoge Temperaturregelung eines GC mit Halogenlampenheizung,” Studienarbeit, Technical University of Hamburg-Harburg, Dept. of Measurement Engineering.
Retention Indices. <URL:www.plant-hormones. info/retentionindex.htm>
Rich Neswold, 2001, “GNU Development Environment for the AVR Microcontroller,” <URL: www.avrfreaks.net>.
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Banik, R., Lee, DY. & Gweon, DG. A high-speed miniature screening gaschromatograph with flame ionization detector. J Mech Sci Technol 19, 2197–2204 (2005). https://doi.org/10.1007/BF02916459
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DOI: https://doi.org/10.1007/BF02916459