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Synthesis of rosinimide modified with polyphenylpyridinylsiloxane and its characteristics

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Abstract

Rosin maleic anhydride adduct (RMA)-bisester was prepared by the esterification of chlorinated RMA with hydroquinone. Phenylpyridinylcyclotrisiloxane (D Ph,Py3 ) was synthesized from phenylpyridinyldichlorosilane in the presence of zinc oxide catalyst, and amino group terminated polyphenylpyridinylsiloxane prepolymer was prepared by equilibrium polymerization of D Ph,Py3 with 1,3-bis(3-aminopropyl)-1,1,3,3-tetramethyldisiloxane. Rosinimide (PSMR) was prepared from the imidization of RMA-bisester with polyphenylpyridinylsiloxane prepolymer at 120°C for 7 h using γ-butyrolactone/pyridine. It showed that PSMR had better thermal stalbility than rosinimide modified with polydimethylsiloxane.

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Authors and Affiliations

  1. Hyperstructured Organic Materials Research Center, Department of polymer Science & Engineering, Dankook University, 140-714, Seoul, Korea

    Doo Whan Kang & Young Min Kim

  2. Department of Chemical Engineering, Dankook University, 140-714, Seoul, Korea

    Young Min Kim

Authors
  1. Doo Whan Kang
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  2. Young Min Kim
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Correspondence to Doo Whan Kang.

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Kang, D.W., Kim, Y.M. Synthesis of rosinimide modified with polyphenylpyridinylsiloxane and its characteristics. Fibers Polym 1, 67–70 (2000). https://doi.org/10.1007/BF02875187

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  • DOI: https://doi.org/10.1007/BF02875187

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