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Theoretical and experimental researches of size effect in micro-indentation test

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Abstract

Micro-indentation tests at scales on the order of sub-micron have shown that the measured hardness increases strongly with the indent depth or indent size decreasing, which is frequently referred to as the size effect. However, the trend is at odds with the size-independence implied by conventional elastic-plastic theory. In this paper, strain gradient plasticity theory is used to model the size effect for materials undergoing the micro-indenting. Meanwhile, the micro-indentation experiments for single crystal copper and single crystal aluminum are carried out. By the comparison of the theoretical predictions with experimental measurements, the micro-scale parameter of strain gradient plasticity theory is predicted, which is fallen into the region of 0.8–1.5 micron for the conventional metals such as copper (Cu), aluminum (Al) and silver (Ag). Moreover, the phenomena of the pile-up and sink-in near micro-indent boundary are investigated and analyzed in detail.

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References

  1. Nix, W. D., Gao, H., Indentation size effects in crystalline materials: a law for strain gradient plasticity, J. Mech. Phys. Solids, 1998, 46(3): 411.

    Article  MATH  Google Scholar 

  2. McElhaney, K. W., Vlassak, J. J., Nix, W. D., Determination of indenter tip geometry and indentation contact area for depth-sensing indentation experiments, J. Mater. Res., 1998, 13(5): 1300.

    Article  Google Scholar 

  3. Begley, M., Hutchinson, J. W., The mechanics of size-dependent indentation, J. Mech. Phys. Solids, 1998, 46: 1029.

    Google Scholar 

  4. Shu, J. Y., Fleck, N. A., The prediction of a size effect in micro-indentation, Int. J. Solids Structures, 1998, 35(13): 1363.

    Article  MATH  Google Scholar 

  5. Poole, W. J., Ashby, M. F., Fleck, N. A., Micro-hardness tests on annealed and work-hardened copper polycrystals, Scripta Metal1 Mater, 1996, 34: 559.

    Article  Google Scholar 

  6. Atkinson, M., Further analysis of the size effective in indentation hardness tests of some metals, J. Mater. Res., 1995, 10: 2908.

    Article  Google Scholar 

  7. Ma, Q., Clarke, D. R., Size dependent hardness of silver single crystals, J. Mater. Res., 1995, 10: 853.

    Article  Google Scholar 

  8. Stelmashenko, N. A., Walls, M. G., Brown, L. M. et al., Microindentation on W and Mo priented single crystals: an STM study, Acta Metall Mater, 1993, 41: 2855.

    Article  Google Scholar 

  9. Cheng, Y. T., Cheng, C. M., Scaling relationships in conical indentation of elastic-perfectly plastic solids, Int. J. Solids Structures, 1999, 36: 1231.

    Article  MATH  Google Scholar 

  10. Fleck, N. A., Hutchinson, J. W., Strain gradient plasticity, in Advances in Applied Mechanics (eds. Hutchinson, J. W., Wu, T. Y.), 1997, 33: 295.

    Article  Google Scholar 

  11. Gao, H., Huang, Y., Nix, W. D. et al., Mechanism-based strain gradient plasticity - I, Theory. J Mech Phys Solids, 1999, 47: 1239.

    Article  MATH  MathSciNet  Google Scholar 

  12. Aifantis, E. C., On the microstructural origin of certain inelastic models, Trans. ASME J. Eng. Mater. Tech., 1984, 106: 326.

    Article  Google Scholar 

  13. Wei, Y., Hutchinson, J. W., Steady-state crack growth and work of fracture for solids characterized by strain gradient plasticity, J. Mech. Phys. Solids, 1997, 45(8): 1253.

    Article  MATH  MathSciNet  Google Scholar 

  14. Timoshenko, S. P., Goodier, J. N., Theory of Elasticity, 3rd ed., New York: McGraw-Hill, Inc., 1970, 401.

    MATH  Google Scholar 

  15. Shaw, M. C, In Mechanical Behavior of Materials (eds. McClintock, F. A., Argon, A. S.), Reading: Addison-Wesley, 1966, 443.

    Google Scholar 

  16. Xia, Z. C., Hutchinson, J. W., Crack tip fields in strain gradient plasticity, J. Mech. Phys. Solids, 1996, 44: 1621.

    Article  Google Scholar 

  17. Chen, J. Y., Wei, Y., Huang, Y. t a1., The crack tip fields in strain gradient plasticity: the asymptotic and numerical analyses, Eng. Fract. Mech., 1999, 64: 625.

    Article  Google Scholar 

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Correspondence to Yueguang Wei.

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Wei, Y., Wang, X., Wu, X. et al. Theoretical and experimental researches of size effect in micro-indentation test. Sci. China Ser. A-Math. 44, 74–82 (2001). https://doi.org/10.1007/BF02872285

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  • DOI: https://doi.org/10.1007/BF02872285

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