Skip to main content
Log in

Differences in microstructure of Pd77.5Au6Si16.5 alloy solidified under microgravity and gravity conditions

  • Published:
Science in China Series A: Mathematics Aims and scope Submit manuscript

Abstract

The microstructure of Pd77.5Au6Si16.5alloy solidified both on board a Chinese Retrievable Satellite and on the earth is studied. Postmortem analyses of microstructure presented that the same types of phases, primary phase (Pd3Si) and eutectics (Pd3Si + Pd solid solution) were formed in both cases. But the phase morphologies were quite different. It was dendritic for the primary phase and lamellar for the eutectics under normal gravity condition. However, under microgravity condition the primary phase was granular and the eutectic was peculiar network. Detailed analysis showed that the differences in morphologies of the microstructure were due to the existence of gravity-induced buoyancy convection on the earth which increased the mass transport abilities and decreased the thickness of the solute boundary in front of the solid-liquid interface during solidification under normal gravity condition.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Rex, S., Convective aspects of solidification experiments under low gravity, inInteractive Dynamics of Convection and Solidification (ed. Davis, S. H.), Netherlands: Kluwer Academic Publishers, 1992, 159–193.

    Google Scholar 

  2. Glicksman, M. E., Koss, M. Winsa, E.A., The chronology of a microgravity spaceflight experiment: IDGE,JOM, 1995, 47(8): 49.

    Google Scholar 

  3. Nguyen Thi, H., Li, Q., Billia, B. et al., Preliminary results of D-2 MEDEA-DENSO experiments on directional solidification of Al-Li alloys, inProceeding of the Norderney Symposium on Scientific Results of the German Spacelab Mission D-2, Norderney, Germany, March, 1994, 379–385.

    Google Scholar 

  4. Stehle, M., Rex, S., Controlled mass transport during directional solidification experiments of a thermosolutally unstable CuMn alloy, inProceeding of the Norderney Symposium on Scientific Results of the German Spacelab Mission D-2, Norderney: DCR, 1994, 386–393.

  5. Liu, R. P., Sun, L. L., Zhao, J. H. et al., Evaluation of effective mass transport coefficients trough comparison of solidification on the ground and on board a satellite,Appl. Phys. Lett., 1997, 71: 64.

    Article  Google Scholar 

  6. Liu, R. P., Sun, L. L., Wang, W. K. et al., Solidification characteristics of Pd40Ni40P20 alloy under microgravity condition,Science in China, Ser. A, 1997, 40: 662.

    Article  Google Scholar 

  7. Rex, S., Solidification: A multidisciplinary and stimulating microgravity research field to get over barriers of materials production, inProceeding of the Norderney Symposium on Scientific Results of the German Spacelab Mission D-2, Norderney, Germany, March, 1994, 359–365.

    Google Scholar 

  8. Steinberg, J., Lacy, L. L., John, J., Production of bulk amorphous Pd77.5CuuSi16.5 in a containerless low-gravity environment,Appl. Phys. Lett., 1981, 38: 135.

    Article  Google Scholar 

  9. Chen, H. S., Miller, C. E., A rapid quenching technique for the preparation of thin uniform films of amorphous solids,Rev. Sci. Instr., 1970, 41: 1237.

    Article  Google Scholar 

  10. Sun, L. L., Wu, Q., Wang, W. K., Decomposition of metastable phase and formation of amorphous silicon in Pd77.5Au6Si16.5 Alloy,J. Mat. Sci. Lett., 1996, 15: 922.

    Article  Google Scholar 

  11. Mao, Z. L., Wang, W. K., Phase formation in drop-tube processing from undercooled PdAuSi melt,J. Mater. Sci., 1993, 28: 4 850.

    Article  Google Scholar 

  12. Sun, L. L., Wu, Q., Wang, W. K., Microstructure of PdAuSi alloy droplet solidified in a drop-tube processing,J. Mater. Sci. Technol., 1996, 12: 385.

    Google Scholar 

  13. Liu, R. P.,Ph. D. Dissertation (in Chinese), Beijing: Institute of Physics, Chinese Academy of Sciences, 1998, 45–80.

    Google Scholar 

  14. Hu, H. Q.,Metal Solidification (in Chinese), Beijing: Metallurgical Industrial Press, 1985, 149–214.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Liu, R., Zhao, J., Zhang, X. et al. Differences in microstructure of Pd77.5Au6Si16.5 alloy solidified under microgravity and gravity conditions. Sci. China Ser. A-Math. 42, 74–79 (1999). https://doi.org/10.1007/BF02872052

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02872052

Keywords

Navigation